GC Analysis of Basic Drugs on SLB®-5ms (20 m x 0.18 mm I.D., 0.36 μm) after SPME using 65 μm PDMS/DVB Fiber, Fast GC Analysis
材料
SPMEファイバー
製品番号
詳細
価格
SPMEファイバー・ポリジメチルシロキサン／ジビニルベンゼン（PDMS/DVB）
df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with manual holderCONDITIONS
sample/matrix
500 μg/L of each compound in 2 mL 0.05M phosphate buffer, 25% sodium chloride, pH=11
SPME fiber
Polyacrylate, 85 μm (57304); PDMS/DVB Stableflex, 65 μm (57326-U)
extraction
15 min, fiber immersion in water, room temperture, stirring at 450 rpm
desorption process
2 min, 250 °C
column
SLB-5ms, 20 m x 0.18 mm I.D., 0.36 μm (28576-U)
oven
100 °C (1 min), 20 °C/min to 325 °C (5 min)
detector
MSD, m/z 40 - 450
MSD interface
325 °C
carrier gas
helium, 1.5 mL/min, constant
liner
0.75 mm I.D. SPME
詳細
法的情報
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany