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GC Analysis of FAMEs in Peanuts on Omegawax

GC Analysis of FAMEs in Peanuts on Omegawax suitable for GC

材料

分析カラム

製品番号
詳細
価格

OmegawaxキャピラリーGCカラム

L × I.D. 30 m × 0.25 mm, df 0.25 μm

関連製品

製品番号
詳細
価格

Aldrich® 一口丸底フラスコ

capacity 50 mL, joint: ST/NS 24/40

Aldrich® modified Friedrichs condenser with SafetyBarb® tubing connectors

jacket O.D. 37 mm, Overall H 270 mm

Aldrich® modified Friedrichs condenser with SafetyBarb® tubing connectors

jacket O.D. 37 mm, Overall H 420 mm

Aldrich® modified Friedrichs condenser with SafetyBarb® tubing connectors

jacket O.D. 54 mm, Overall H 300 mm

BF3-メタノール

10 % (w/w)

CONDITIONS

column

OMEGAWAX 250, 30 m x 0.25 mm I.D., 0.25 μm (24136)

oven

170 °C, 1 °C/min to 225 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 1.2 mL/min constant flow

injection

1 μL, split 100:1

liner

4 mm ID FocusLiner w/taper

sample

Dry roasted, unsalted peanuts prepared for analysis per AOCS Official Method Ce 1k-09

詳細

アナリシスノート

This application illustrates the extraction and GC analysis of peanuts for fatty acids. The health benefits of peanuts and peanut oil are associated with their high oleic acid content. Oleic acid is believed to help lower cholesterol and reduce the risk of heart disease. Oleic acid, also found in olive oil, is a major contributor to the health benefits associated with the “Mediterranean Diet.”
The samples were prepared using acid digestion /alkali hydrolysis followed by methylation as described in AOCS Official Method Ce 1k-09. BHT was added as an antioxidant prior to extraction. All samples were concentrated to 1 mL prior to GC analysis. The Omegawax GC column was used in the analysis of the saturated and unsaturated fatty acids present in the sample.

法的情報

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