GC Analysis of Class 3 Residual Solvents on SUPELCOWAX 10

column

SUPELCOWAX 10, 30 m x 0.53 mm I.D., 1.0 μm (25301-U)

oven

35 °C (15 min), 5 °C/min to 200 °C

inj. temp.

225 °C

detector

FID, 250 °C

carrier gas

helium, 30 cm/sec @ 35 °C

injection

1.0 μL 33:1 split

liner

single taper

sample

27 analytes, each at 3000 μg/mL in methanol