EN Method 2005/108/EC: GC Analysis of Pesticide/PAH Compounds on SLB^®-5ms

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

50 °C (3 min), 25 °C/min to 250 °C (3 min), 4 °C/min to 325 °C (5 min)

inj. temp.

300 °C

MSD interface

300 °C / 200 °C (source/quads)

scan range

SIM

carrier gas

helium, 0.9 mL/min constant

injection

0.5 μL, pulsed (15 psi until 0.20 min) splitless (1.0 min)

liner

2 mm I.D. FocusLiner^™ inlet liner with taper

sample

26 analytes at 50 ppb each in methylene chloride