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テクニック
HPLC: suitable
試験パラメータ
column: Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U)
gradient: 5 mM ammonium formate in acetonitrile:water (90:10, v/v)
flow rate: 0.4 mL/min
column temp.: 35 °C
detector: TOF/MS
injection: 2 μL
sample: 300 ng/mL in acetonitrile
適合性
application for HPLC
アプリケーション
forensics and toxicology
アナリシスノート
The fluoroamphetamines (FA) are a group of "designer" stimulant drugs in amphetamine family. The rapid LC/MS analysis of four members of the FA family on Ascentis Express HILIC is shown here. Cerilliant CRMs were used to ensure reliable MS identification and quantification.
法的情報
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany
アナライト
詳細
(±)-2-Fluoroamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
4-Fluoroamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
(±)-2-Fluoromethamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
(±)-4-Fluoromethamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
分析カラム
標準
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試験成績書（COA）
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