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Merck

CRM44794

Supelco

ホスファミドン

certified reference material, TraceCERT®, Manufactured by: Sigma-Aldrich Production GmbH, Switzerland

別名:

2-クロロ-N,N-ジエチル-3-(ジメチルホスホノ)クロトン酸 アミド

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About This Item

実験式(ヒル表記法):
C10H19ClNO5P
CAS番号:
分子量:
299.69
Beilstein:
8323501
MDL番号:
UNSPSCコード:
41116107
NACRES:
NA.24

グレード

certified reference material
TraceCERT®

品質水準

製品種目

TraceCERT®

シェルフライフ

limited shelf life, expiry date on the label

メーカー/製品名

Manufactured by: Sigma-Aldrich Production GmbH, Switzerland

フォーマット

neat

保管温度

−20°C

SMILES記法

CCN(CC)C(=O)\C(Cl)=C(\C)OP(=O)(OC)OC

InChI

1S/C10H19ClNO5P/c1-6-12(7-2)10(13)9(11)8(3)17-18(14,15-4)16-5/h6-7H2,1-5H3/b9-8+

InChI Key

RGCLLPNLLBQHPF-CMDGGOBGSA-N

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詳細

This certified reference material (CRM) is produced and certified in accordance with ISO/IEC 17025 and ISO 17034. This CRM is traceable to primary material from an NMI, e.g. NIST or NMIJ.
Certified content by quantitative NMR incl. uncertainty and expiry date are given on the certificate.
Download your certificate at: http://www.sigma-aldrich.com
Phosphamidon is a broad-spectrum systemic organophosphorus pesticide. It is used as an insecticide against sap-feeding insects, rice-stem borers, and rice leaf beetles in crops of sugarcane, citrus fruits, commercial cotton, and nuts.
As per Regulation (EC) No. 1107/2009, repealing directive 91/414/EEC, phosphamidon is not approved for use in the European Union. But a default maximum residue limit (MRL) of 0.01 mg/kg is applicable for the presence of phosphamidon in products of plant origin, in accordance with Regulation (EC) No. 149/2008.

アプリケーション

The certified reference material (CRM) is intended to be used as a calibrant for chromatography and other analytical techniques.
The phosphamidon CRM may also find following uses:
  • Determination of five organophosphorus pesticides in a medicinal herb sample using QuEChERS along with dispersive liquid-liquid microextraction (DLLME) and stacking followed by micellar electrokinetic chromatography (MEKC)
  • Magnetic solid phase microextraction (MSPE) of five organophosphorus pesticides using graphene based cyanopropyltriethoxysilane as an adsorbent from cow′s milk samples and their subsequent determination by gas chromatography with micro-electron capture detector
  • Investigation of residue levels of highly toxic pesticides in 6554 samples of fruits and vegetables by quadrupole time-of-flight LC/MS
  • Analysis of 4 organophosphorus pesticides by gas chromatography with microelectron capture detector following their extraction using a newly synthesized magnetic hybrid material as a solid phase extraction adsorbent
  • Multi-residue analysis of 44 organophosphorus pesticides by QuEChERS method combined with gas chromatography in Pogostemon cablin samples
  • Detection of organophosphorus pesticides in Chinese cabbage sample by a newly designed positive photoionization-ion mobility spectrometry (PP-IMS) apparatus

法的情報

TraceCERT is a registered trademark of Merck KGaA, Darmstadt, Germany

ピクトグラム

Skull and crossbonesHealth hazardEnvironment

シグナルワード

Danger

危険有害性情報

危険有害性の分類

Acute Tox. 2 Oral - Acute Tox. 3 Dermal - Aquatic Acute 1 - Aquatic Chronic 1 - Muta. 2

保管分類コード

6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

WGK

WGK 3

引火点(°F)

Not applicable

引火点(℃)

Not applicable


適用法令

試験研究用途を考慮した関連法令を主に挙げております。化学物質以外については、一部の情報のみ提供しています。 製品を安全かつ合法的に使用することは、使用者の義務です。最新情報により修正される場合があります。WEBの反映には時間を要することがあるため、適宜SDSをご参照ください。

労働安全衛生法名称等を表示すべき危険物及び有害物

名称等を表示すべき危険物及び有害物

労働安全衛生法名称等を通知すべき危険物及び有害物

名称等を通知すべき危険物及び有害物

Jan Code

CRM44794-100MG:
CRM44794-BULK:


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試験成績書(COA)

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以前この製品を購入いただいたことがある場合

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文書ライブラリにアクセスする

Trace determination of five organophosphorus pesticides by using QuEChERS coupled with dispersive liquid-liquid microextraction and stacking before micellar electrokinetic chromatography
Wei J, et al.
Analytical Methods : Advancing Methods and Applications, 7(14), 5801-5807 (2015)
Magnetic graphene-based cyanopropyltriethoxysilane as an adsorbent for simultaneous determination of polar and non-polar organophosphorus pesticides in cow?s milk
Nodeh H R, et al.
Royal Society of Chemistry Advances, 6(30), 24853-24864 (2016)
Qinghua Zhou et al.
Talanta, 176, 247-252 (2017-09-18)
Ion mobility spectrometry (IMS) opened a potential avenue for the rapid detection of organophosphorus pesticides (OPPs), though an improved selectivity of stand-alone IMS was still in high demand. In this study, a stand-alone positive photoionization ion mobility spectrometry (PP-IMS) apparatus
Photocatalytic degradation of phosphamidon using Ag-doped ZnO nanorods
Korake PV, et al.
Toxicological & Environmental Chemistry, 94(6), 1075-1085 (2012)
Somayeh Koupaei Malek et al.
Journal of separation science (2018-06-08)
The precise control of pesticide residues in foodstuffs depends significantly on the clean extraction of analytes using specifically designed separation methods. In this study, a one-pot sol-gel process was used for the preparation of a magnetic hybrid silica gel tetraethylortho

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