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G006109

GC Analysis of Sulfur Compounds in Gasoline on SPB®-1 SULFUR

suitable for GC

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About This Item

tecniche

gas chromatography (GC): suitable

Parametri analitici

column: SPB-1 SULFUR, 30 m x 0.32 mm I.D., 4.0 μm (24158)
oven: 35 ºC, 5 ºC/min to 200 ºC
inj. temp.: 275 °C
detector: FID, 300 ºC; FPD, 300 ºC
carrier gas: helium, 20 cm/sec
injection: 1 μL 100:1 split
sample: Gasoline

applicazioni

petroleum

Risultati analitici

Two issues must be overcome for the analysis of sulfur compounds in fuels. 1) Detection of these compounds in a hydrocarbon sample matrix, and 2) adsorption of these compounds by the column. Sulfur specific detectors, such as a flame photometric detector (FPD), can be used to overcome the first challenge. A low phase ratio column, such as the SPB-1 SULFUR, can be used to overcome the second challenge. This slide shows the analysis of a gasoline sample, in which the column effluent was split to two detectors. The top chromatogram shows the FID response, and the bottom chromatogram shows the FPD response.

Note legali

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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