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Merck
  • Development of a rapid and accurate method for the determination of key compounds of pig odor.

Development of a rapid and accurate method for the determination of key compounds of pig odor.

Journal of chromatography. A (2004-07-06)
Stephanie Willig, Markus Lacorn, Rolf Claus
摘要

Sampling of odor substances in the emissions from swine production facilities is still the limiting step for routine odor quantification. Solid sorption techniques based on cartridges were developed for three categories of substances (indoles, volatile fatty acids and methylthiol) and were standardized to a sampling time of 15 min. These cartridges also trap dust particles which transport odor substances. Quantification was performed by RP-HPLC or GC. Reliability criteria revealed excellent values for sensitivity (lower ppb level) and repeatability (R.S.D. < 10%), thus they are comparable to fiber solid-phase micro extraction sorption techniques. Parallel determinations in feces and air revealed high correlations (r = 0.99, P < 0.01), so that microbial processes during digestion determine odor quality and hence provide a possibility to reduce odor via feeding.

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Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, StableFlex
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, for use with manual holder
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with autosampler
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with manual holder or autosampler, fiber L 2 cm
Supelco
SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, StableFlex, for use with autosampler
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SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, needle size 24 ga, for use with manual holder
Supelco
SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 23 ga
Supelco
SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 24 ga
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, for use with manual holder, needle size 24 ga
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 23 ga, StableFlex, for use with autosampler
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with manual holder
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 24 ga, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, StableFlex, for use with autosampler
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聚丙烯酸酯 (PA) 固相微萃取萃取头, df 85 μm(PA, for use with autosampler, needle size 23 ga
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 23 ga, PDMS/DVB StableFlex, for use with autosampler
Supelco
聚丙烯酸酯 (PA) 固相微萃取萃取头, df 85 μm(PA, for use with autosampler, needle size 24 ga
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, for use with manual holder, StableFlex fiber
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with manual holder
Supelco
SPME 纤维组件聚二甲基硅氧烷 (PDMS), df 100 μm(PDMS, for use with manual holder, needle size 23 ga
Supelco
SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with autosampler
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with autosampler
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固相微萃取 StableFlex 萃取头组合套件, for use with manual holder
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Carbowax-聚乙二醇 (PEG) 固相微萃取萃取头, needle size 23 ga, df 60 μm(PEG, for use with autosampler
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SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), df 65 μm(PDMS/DVB, for use with autosampler, needle size 23 ga
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with manual holder
Supelco
固相微萃取 StableFlex 萃取头组合套件, needle size 23 ga, for use with autosampler
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SPME固相微萃取萃取头,二甲基硅氧烷/二乙烯基苯(PDMS/DVB), fused silica fiber, df 65 μm(PDMS/DVB, for use with manual holder, needle size 23 ga
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SPME 纤维分类套件 4, for use with manual holder, size 24 ga
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聚丙烯酸酯 (PA) 固相微萃取萃取头, df 85 μm(PA, for use with manual holder, needle size 24 ga