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Merck
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文件

16898

Supelco

次乌头碱

analytical standard

别名:

16,16-trimethoxy-4-(methoxymethyl)-20-methyl-,8-acetate benzoate,(1-α,6-α,14-α,15-α,16-β)-aconitane-8,13,14,15-tetraol

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About This Item

经验公式（希尔记法）:
C33H45NO10
CAS号:
6900-87-4
分子量:
615.71
分類程式碼代碼:
12352200
NACRES:
NA.24

等級

analytical standard

化驗

≥97.5% (HPLC)

光學活性

[α]/D 22.5±2.5°, c = 0.1 in chloroform

儲存期限

limited shelf life, expiry date on the label

格式

neat

儲存溫度

2-8°C

SMILES 字串

O=C(C1=CC=CC=C1)O[C@H]2[C@@]3(O)[C@@H](OC)[C@H](O)[C@]4(OC(C)=O)C5[C@H](OC)C6C([C@@H](OC)CC[C@]6(CN7C)COC)(C75)[C@H](C3)C42

InChI

1S/C33H45NO10/c1-17(35)44-33-21-19(14-31(38,28(42-6)26(33)36)27(21)43-29(37)18-10-8-7-9-11-18)32-20(40-4)12-13-30(16-39-3)15-34(2)25(32)22(33)23(41-5)24(30)32/h7-11,19-28,36,38H,12-16H2,1-6H3/t19-,20+,21?,22?,23+,24?,25?,26+,27-,28+,30+,31-,32?,33-/m1/s1

InChI 密鑰

FIDOCHXHMJHKRW-XCIBRDTCSA-N

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一般說明

Hypaconitine is a constituent of diester-diterpene Aconitum alkaloids (AAs), which are found in aconite plants.

應用

Hypaconitine may be used as an analytical standard for the determination of the analyte in biological samples, Aconitum tubers by liquid chromatography (LC) based techniques.

象形圖

Skull and crossbones
GHS06

訊號詞

Danger

危險聲明

H300 + H330

危險分類

Acute Tox. 2 Inhalation - Acute Tox. 2 Oral

儲存類別代碼

6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

水污染物質分類（WGK）

WGK 2

閃點（°F）

Not applicable

閃點（°C）

Not applicable

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分析证书(COA)

Lot/Batch Number
BCBZ6608
BCBW6149
BCBR8710
26599973
74464276

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Rina Kaneko et al.
Journal of mass spectrometry : JMS, 41(6), 810-814 (2006-06-14)
The Aconitum species (Ranunculaceae) are widely distributed in northern Asia and North America. Their roots are popularly used in herbal medicines in China and Japan. Many cases of accidental, suicidal and homicidal intoxication with this plant have been reported; some
Ying Xie et al.
Journal of chromatography. A, 1093(1-2), 195-203 (2005-10-20)
By optimizing the extraction, separation and analytical conditions, a reliable and accurate high-performance liquid chromatography (HPLC) method coupled with photodiode array detector (DAD) was developed for simultaneous quantitative determination of six Aconitum alkaloids, i.e., aconitine, mesaconitine, hypaconitine, benzoylaconine, benzoylmesaconine and
Lei-ping He et al.
Journal of analytical toxicology, 33(9), 588-594 (2009-12-31)
A rapid, sensitive, and specific liquid chromatography-electrospray ionization-tandem mass spectrometry (LC-ESI-MS-MS) method was developed and validated for simultaneous determination of aconitine (AC), mesaconitine (MA), and hypaconitine (HA), the three toxic constituents from Sini decoction (SND) in rat plasma. After the
Simultaneous quantitation of aconitine, mesaconitine, hypaconitine, benzoylaconine, benzoylmesaconine and benzoylhypaconine in human plasma by liquid chromatography-tandem mass spectrometry and pharmacokinetics evaluation of ?SHEN-FU? injectable powder
Zhang F, et al.
Journal of Chromatography. B, Biomedical Applications, 873(2), 173-179 (2008)
Simultaneous analysis of aconitine, mesaconitine, hypaconitine, and jesaconitine in whole blood by LC-MS-MS using a new polymer column
Hattori H, et al.
Forensic Toxicology, 27(1), 7-11 (2009)
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