1.15388

TLC plates, Silica gel 60 RP-8 F₂₅₄s

pkg of 25 plates, plate L × W 20 cm × 20 cm, glass support

• 别名: RP-8 Silica Gel Thin-layer Chromatography Plates
• 分類程式碼代碼: 41115711
• NACRES: NB.21

属性

• 材料: glass support; silica gel 60 matrix
• 品質等級: 100
• 特點: binder Organic Polymer; fluorescent indicator
• 包裝: pkg of 25 plates
• 技術: thin layer chromatography (TLC): suitable
• 層厚度: 250 μm
• 板長度 × 寬度: 20 cm × 20 cm
• 粒徑: 10-12 μm
• 孔徑: 60 Å medium pore diameter
• 儲存溫度: 2-30°C

说明

一般說明

25 Glass plates 20 x 20 cm

RP modified plates serve two purposes: act as a pilot method for HPLC and allow to choose various solvent system for special separations. Our RP-modified silica layers are well suited for many separation challenges that unmodified silica cannot overcome. These layers use aqueous solvent systems to separate extremely non-polar substances and analyze particular polar substances that can adapt to ion-pair chromatography. What’s more, RP-modified silica layers are less dependent on atmospheric humidity. Unlike unmodified silica, RP-phases do not exhibit catalytic activity. This makes them the plates of choice for unstable substance that tend to experience oxidative degradation.

應用

Glass TLC plates, RP-8 modified silica gel coated with flourescent indicator F254s. The RP-8 modified silica gel TLC plates come in a quantity of 25 size 20x20 cm for thin layer chromatography applications.

聯結

Replaces: 15388-7; 15388

分析報告

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m²/g
Pore volume (N₂-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 9.5 - 11.5 µm
Layer thickness: 200 - 270 µm
Deviation of layer thickness per plate: ≤ 35 µm
Chromatographic testings:
A) Cholesterin test
hRf-values
- cholesterin, cholesterin test:
68 - 74
B) Steroid test
- methyltestosterone, steroid test: 45 - 55
- Reichstein S, steroid test: 65 - 75
- hydrocortisone, steroid test: 75 - 91
Typical value determined on an activated plate (120°C, 15 min)
Eluent a) aceton/ water (95/5 v/v)
Eluent b) acetonitrile/ water (70/30 v/v)