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Merck

28467-U

Supelco

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.10 μm

Sinónimos:

GC column, SPB-5, 5% diphenyl, mass spec

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About This Item

Código UNSPSC:
12000000
eCl@ss:
32119290
NACRES:
SB.54

858,00 €


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Materiales

fused silica

Nivel de calidad

Agency

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

cumplimiento norm.

FDA LIB 4423

Parámetros

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

Valor Beta

625

df

0.10 μm

técnicas

GC/MS: suitable
gas chromatography (GC): suitable

L × D.I.

30 m × 0.25 mm

grupo activo de la matriz

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

aplicaciones

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

tipo de columna

capillary non-polar

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Descripción general

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded and highly crosslinked
  • Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
  • ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Aplicación

  • An improved method for cyanide determination in blood using solid-phase microextraction and gas chromatography/mass spectrometry.: This study presents an enhanced method for determining cyanide levels in blood, employing solid-phase microextraction combined with gas chromatography/mass spectrometry. This technique improves sensitivity and accuracy, essential for toxicological and forensic analysis (Frison et al., 2006).
  • Photochemical production of conjugated linoleic acid from soybean oil.: This research explores the photochemical production of conjugated linoleic acid (CLA) from soybean oil. The study utilized gas chromatography for the analysis of CLA, demonstrating an efficient method for producing this valuable compound with potential health benefits (Gangidi & Proctor, 2004).
  • Development of a solid-phase microextraction GC-NPD procedure for the determination of free volatile amines in wastewater and sewage-polluted waters.: This work describes the development of a GC-NPD procedure using solid-phase microextraction for detecting volatile amines in wastewater. This method offers improved detection limits and specificity, which are critical for environmental monitoring and water quality assessment (Abalos et al., 1999).

Otras notas

We offer a variety of chromatography accessories including analytical syringes

Información legal

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Certificados de análisis (COA)

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Alessia Arena et al.
Food chemistry, 396, 133721-133721 (2022-07-24)
Phthalic acid esters (PAEs), known as phthalates, have a variety of industrial applications, mainly related to their ability to increase plastic softness,flexibility, and durability. With regard to toxicological aspects, several studies suggest that phthalates would act as endocrine-disrupting chemicals, and
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction
Annie Xu Zeng et al.
Analytica chimica acta, 803, 166-173 (2013-11-13)
Due to their distinct chemical properties, the application of ionic liquid (IL) compounds as gas chromatography (GC) stationary phases offer unique GC separation especially in the analysis of geometric and positional fatty acid methyl ester (FAME) isomers. Elution behaviour of
Lisa Simonsson et al.
Chemphyschem : a European journal of chemical physics and physical chemistry, 11(5), 1011-1017 (2010-03-20)
We investigate the Ca(2+)-triggered fusion of lipid vesicles site-selectively tethered to a DNA-modified supported lipid bilayer array, with the DNA strands designed such that hybridization occurs in a zipperlike fashion. Prior to the addition of Ca(2+), which is observed to
Sophie Duclos et al.
Proteomics, 11(5), 854-864 (2011-02-01)
The essential roles of the endovacuolar system in health and disease call for the development of new tools allowing a better understanding of the complex molecular machinery involved in endocytic processes. We took advantage of the floating properties of small

Artículos

The analysis of melamine and related compounds in dog food with the use of more economical gas chromatography-mass spectrometry (GC-MS) instrumentation.

Contenido relacionado

This page is intended to make it easier to find the consumables you need based on the analytical method you’re using. Methods included on this page come from the EPA, Standard Methods and ASTM.

Preguntas

1–6 de 6 Preguntas  
  1. What is the Department of Transportation shipping information for this product?

    1 respuesta
    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

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  2. Would you recommend SLB™-5ms Capillary GC Columns for all applications instead of Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S?

    1 respuesta
    1. Yes.

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  3. How does the SLB™-5ms Capillary GC Column differ from our other 5-type columns?

    1 respuesta
    1. Many of our other 5-type columns (Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S) incorporate a siloxane polymer (backbone comprised of Si and O atoms only, side groups are either methyl or phenyl). The SLB-5ms column incorporates a silphenylene polymer (backbone comprised of Si and O atoms plus some phenyl groups, side groups are either methyl or phenyl).

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  4. What are the benefits of the SLB™-5ms Capillary GC Column over other manufacturers’ -5ms columns?

    1 respuesta
    1. The SLB-5ms excels in several performance criteria.· Low Bleed. The highly crosslinked silphenylene polymer chemistry reduces column bleed to a very low level, resulting in greater signal-to-noise level, allowing lower detection levels.· Inertness. The proprietary surface deactivation reduces interactions between analytes and the column surface, resulting in sharper peak shapes, allowing lower detection levels.· Durability. With the highest published maximum allowable operating temperature (MAOT) of any -5ms column, SLB-5ms columns are designed for long life.· Consistency. Innovative manufacturing processes result in decreased column variability, ensuring that the next column is as good as the last.

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  5. Who uses SLB™-5ms Capillary GC Columns?

    1 respuesta
    1. Any analyst with the need for a non-polar column. Some applications include boiling point separations, GC-MS analyses of semivolatiles, and GC-ECD analyses of pesticides/PCBs. It is estimated that non-polar columns account for 51% of the worldwide column market.

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  6. What if my method does not allow me to change to SLB™-5ms Capillary GC Columns?

    1 respuesta
    1. These methods typically specify a 5-type column (DB-5 or equivalent). The SLB-5ms satisfies that requirement.

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