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Merck

25342

Supelco

Columna para GC capilar SP®-5

L × I.D. 15 m × 0.53 mm, df 3.00 μm

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About This Item

Código UNSPSC:
41115710
eCl@ss:
32119290

Materiales

fused silica

Agency

meets requirements for USP G27 and G36

Parámetros

-60-260 °C temperature (isothermal)
-60-280 °C temperature (programmed)

Valor Beta

44

df

3.00 μm

técnicas

gas chromatography (GC): suitable

L × D.I.

15 m × 0.53 mm

grupo activo de la matriz

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

tipo de columna

capillary non-polar

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Descripción general

Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.
Aplicación: Esta columna no polar de uso general proporciona principalmente un orden de elución por punto de ebullición con un ligero aumento en la selectividad, en especial para los compuestos aromáticos.
Código USP: Esta columna cumple los requisitos G27 y G36 de la USP .
Fase:
  • Ligada
  • Poli(difenil al 5 %/dimetil siloxano al 95 %)
Temperatura Límites:
  • ≤0,32 mm D.I., <2 μm: de -60 °C a 320 °C (isotérmica o programada)
  • ≤0,32 mm D.I., ≥2 μm: de -60 °C a 300 °C (isotérmica o programada)
  • ≥0,53 mm D.I., <2 μm: de -60 °C a 300 °C (isotérmica ) o 320 °C (programada)
  • ≥0,53 mm D.I., ≥2 μm: de -60 °C a 260 °C (isotérmica ) o 280 °C (programada)

Aplicación

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. It may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

Otras notas

We offer a variety of chromatography accessories including analytical syringes

Información legal

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
Determination of sterols by capillary column gas chromatography. Differentiation among different types of olive oil: virgin, refined, and solvent-extracted.
Jimenez O and Gonzalez ADV.
Journal of the American Oil Chemists' Society, 73 (12), 1685-1689 (1996)
J Corwin et al.
Cancer, 43(3), 1007-1013 (1979-03-01)
Solitary plasmacytoma of bone (SPB) and extramedullary plasmacytoma (EMPC) are unusual solitary tumors of plasma cell origin. The clinical differences between these tumors and multiple myeloma are the subject of continued study. This review examines the radiotherapy experience at M.
Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave

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