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Supelco

Columna para GC capilar SP®-5

L × I.D. 30 m × 0.53 mm, df 5.00 μm

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About This Item

Código UNSPSC:
41115710
eCl@ss:
32119290

Materiales

fused silica

Agency

meets requirements for USP G27 and G36

Parámetros

-60-260 °C temperature (isothermal)
-60-280 °C temperature (programmed)

Valor Beta

27

df

5.00 μm

técnicas

gas chromatography (GC): suitable

L × D.I.

30 m × 0.53 mm

grupo activo de la matriz

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

tipo de columna

capillary non-polar

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Descripción general

Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.
Aplicación: Esta columna no polar de uso general proporciona principalmente un orden de elución por punto de ebullición con un ligero aumento en la selectividad, en especial para los compuestos aromáticos.
Código USP: Esta columna cumple los requisitos G27 y G36 de la USP .
Fase:
  • Ligada
  • Poli(difenil al 5 %/dimetil siloxano al 95 %)
Temperatura Límites:
  • ≤0,32 mm D.I., <2 μm: de -60 °C a 320 °C (isotérmica o programada)
  • ≤0,32 mm D.I., ≥2 μm: de -60 °C a 300 °C (isotérmica o programada)
  • ≥0,53 mm D.I., <2 μm: de -60 °C a 300 °C (isotérmica ) o 320 °C (programada)
  • ≥0,53 mm D.I., ≥2 μm: de -60 °C a 260 °C (isotérmica ) o 280 °C (programada)

Aplicación

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. It may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

Otras notas

We offer a variety of chromatography accessories including analytical syringes

Información legal

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Certificados de análisis (COA)

Lot/Batch Number
287351-08
287351-07
287351-06
287351-05
287351-04

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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave
Zhihua Fan et al.
Environmental science & technology, 40(19), 6051-6057 (2006-10-21)
A sensitive, simple, and cost-effective passive sampling methodology was developed to quantify personal exposure to gaseous polycyclic aromatic hydrocarbons (PAHs). A Fan-Lioy passive PAH sampler (FL-PPS) is constructed from 320 sections of 1-cm long SPB-5 GC columns (0.75-mm i.d. and
V Gajdůsková et al.
Veterinarni medicina, 37(8), 471-478 (1992-08-01)
Occurrence of individual polychlorinated biphenyl (PCB) congeners in the environment, foodstuffs and other biological materials was assessed. Analysis of specific PCB congeners (28, 52, 101, 138, 153, 180), occurring in animal raw materials and foodstuffs most frequently, has been implemented.
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
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