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55408-U

Supelco

Supel QuE QuEChERS tube

Z-Sep+ Tube, centrifuge tube volume 2 mL, pack of 100 ea

Synonyma:

QuEChERS

Přihlásitk zobrazení cen stanovených pro organizaci a smluvních cen


About This Item

UNSPSC Code:
41115712
NACRES:
NB.21

Název produktu

Supel QuE, Z-Sep+ Tube, centrifuge tube volume 2 mL, pack of 100 ea

material

polypropylene tube

Quality Level

product line

Supel

composition

Z-Sep+, 75 mg

packaging

pack of 100 ea

technique(s)

QuEChERS: suitable

centrifuge tube volume

2 mL

matrix active group

zirconia-based phase

application(s)

food and beverages

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General description

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Other Notes

Supel QuE Z-Sep products enhance sample cleanup for complex matrices by effectively removing more fat and color from sample extracts than traditional phases for QuEChERS methods. By eliminating problematic matrix interferences, Z-Sep products provide more robust LC-MS and GC-MS methods. This proprietary technology can replace C18 and PSA in your current methods without additional method development.

Z-Sep+ is recommended for cleanup of samples containing greater than 15% fat.
Z-Sep/C18 is recommended for cleanup of samples containing less than 15% fat.
Z-Sep is recommended for cleanup of samples prior to analysis of hydrophobic analytes.

Legal Information

Certain uses of this product may be covered by the claims of one or more pending patent applications. For licensing inquiries please contact [email protected]
AOAC is a registered trademark of AOAC International
Supel is a trademark of Sigma-Aldrich Co. LLC

Storage Class

11 - Combustible Solids

wgk_germany

nwg

flash_point_f

Not applicable

flash_point_c

Not applicable


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Anna Laura Capriotti et al.
Journal of chromatography. A, 1343, 69-78 (2014-04-22)
A sensitive, simple and rapid method for the simultaneous determination of 19 mycotoxins in biscuits (a dry matrix containing cereals and egg) has been developed using high performance liquid chromatography coupled to tandem mass spectrometry with electrospray source working in
An overview of analytical methods and occurrence of benzotriazoles, benzothiazoles and benzenesulfonamides in the environment
Herrero, P., et al.
TrAC, Trends in Analytical Chemistry, 62, 46-55 (2014)
Determination of toxic substances, pesticides and mycotoxins, in ginkgo biloba nutraceutical products by liquid chromatography Orbitrap-mass spectrometry
Martinez-Dominguez, G., et al.
Microchemical Journal, Devoted to the Application of Microtechniques in All Branches of Science, 118, 124-130 (2015)
Ana Lozano et al.
Talanta, 118, 68-83 (2013-11-28)
Two sorbents containing ZrO₂ (Z-Sep and Z-Sep+) were tested as a d-SPE clean-up in combination with the QuEChERS and ethyl acetate multiresidue method in the pesticide residues extraction in avocado. All extracts were analysed using gas chromatography coupled with a
Łukasz Rajski et al.
Journal of chromatography. A, 1304, 109-120 (2013-07-23)
Several extraction methods were evaluated in terms of recoveries and extraction precision for 113 pesticides in avocado: QuEChERS with various d-SPE clean-ups (Z-Sep, Z-Sep+, PSA+C18 and silica), miniLuke and ethyl acetate. Extracts were analysed using liquid chromatography coupled with triple

Sortimentní položky

Use QuEChERS methods to analyze samples of milk for veterinary drugs.

Pistachios 45% fat complicates pesticide analysis. But Z-Sep+ sorbent cleanup after QuEChERS extraction can reduce background for reliable results.

Assessment of clean-up sorbents for extracting PAHs from salmon and PCBs from milk, optimized for GC analysis with MS and ECD detection.

Protokoly

A short abstract on a method using QuEChERS and GC/MS/MS for determination of fipronil & fipronil sulfone.

Související obsah

Z-Sep sorbents improve fat and pigment extraction in QuEChERs solid phase extraction for sample preparation.

Náš tým vědeckých pracovníků má zkušenosti ve všech oblastech výzkumu, včetně přírodních věd, materiálových věd, chemické syntézy, chromatografie, analytiky a mnoha dalších..

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