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I7632

Sigma-Aldrich

Iodobenzene

98%

Sinonimo/i:

1-Iodobenzene, 4-Iodobenzene, Benzene iodide, Phenyl iodide

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About This Item

Formula empirica (notazione di Hill):
C6H5I
Numero CAS:
591-50-4
Peso molecolare:
204.01
Beilstein:
1446140
Numero CE:
209-719-6
Numero MDL:
MFCD00001029
Codice UNSPSC:
12352100
ID PubChem:
24896121
NACRES:
NA.22
Prezzi e disponibilità al momento non sono disponibili

Livello qualitativo

200

Saggio

98%

Indice di rifrazione

n20/D 1.62 (lit.)

P. ebollizione

188 °C (lit.)

Punto di fusione

−29 °C (lit.)

Densità

1.823 g/mL at 25 °C (lit.)

Stringa SMILE

Ic1ccccc1

InChI

1S/C6H5I/c7-6-4-2-1-3-5-6/h1-5H
SNHMUERNLJLMHN-UHFFFAOYSA-N

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Categorie correlate

Descrizione generale

Iodobenzene, also known as phenyl iodide, is commonly used as an arylating agent in various cross-coupling reactions.[1][2][3]

Applicazioni

Iodobenzene is used in various C-C coupling reactions.[4][5][6] It can be used in the preparation of iodobenzene dichloride, which is employed as an oxidant to oxidize alcohols to carbonyl compounds[7] and as a chlorinating agent.[8]

Pittogrammi

Exclamation mark
GHS07

Avvertenze

Warning

Indicazioni di pericolo

H302

Classi di pericolo

Acute Tox. 4 Oral

Codice della classe di stoccaggio

10 - Combustible liquids

Classe di pericolosità dell'acqua (WGK)

WGK 3

Punto d’infiammabilità (°F)

170.6 °F - closed cup

Punto d’infiammabilità (°C)

77 °C - closed cup

Dispositivi di protezione individuale

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter

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Certificati d'analisi (COA)

Lot/Batch Number
BCCM7399
BCCL9575
BCCL1457
BCCJ3240
BCCF2534

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Copper(I) iodide purum, ≥99.5%

Sigma-Aldrich

03140

Copper(I) iodide

1-Chloro-4-iodobenzene 99%

Sigma-Aldrich

101605

1-Chloro-4-iodobenzene

Bromobenzene ≥99.5% (GC)

Sigma-Aldrich

16350

Bromobenzene

4-tert-Butyliodobenzene 98%

Sigma-Aldrich

411205

4-tert-Butyliodobenzene

[Bis(trifluoroacetoxy)iodo]benzene 97%

Sigma-Aldrich

232130

[Bis(trifluoroacetoxy)iodo]benzene

Phenylacetylene 98%

Sigma-Aldrich

117706

Phenylacetylene

3-Iodotoluene 99%

Sigma-Aldrich

130737

3-Iodotoluene

4-Iodobenzotrifluoride 97%

Sigma-Aldrich

365858

4-Iodobenzotrifluoride

Phenylboronic acid 95%

Sigma-Aldrich

P20009

Phenylboronic acid

Ring-Opening 1, 3-Dichlorination of Donor-Acceptor Cyclopropanes by Iodobenzene Dichloride.
Garve, Lennart KB et al.
Organic Letters, 16(21), 5804-5807 (2014)
Heck reactions of iodobenzene and methyl acrylate with conventional supported palladium catalysts in the presence of organic and/and inorganic bases without ligands.
Zhao, Fengyu et al.
Chemistry?A European Journal , 6(5), 843-848 (2000)
Iodobenzene dichloride as a stoichiometric oxidant for the conversion of alcohols into carbonyl compounds; two facile methods for its preparation.
Zhao, Xue-Fei and Zhang, Chi
Synthesis, 2007(04), 551-557 (2007)
Size effects of PVP- Pd nanoparticles on the catalytic Suzuki reactions in aqueous solution.
Li, Yin et al.
Langmuir, 18(12), 4921-4925 (2002)
Catalysis by gold (I) and gold (III): a parallelism between homo-and heterogeneous catalysts for copper-free Sonogashira cross-coupling reactions.
Gonzalez-Arellano, Camino et al.
Angewandte Chemie (International Edition in English), 46(9), 1536-1538 (2007)
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Questions

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  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer

    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

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  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer

    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

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