493880

(3aS,7R,7aS)-7,7a-Dihydro-7-hydroxy-2,2-dimethyl-1,3-benzodioxol-4(3aH)-on

0.2 g/mL in 0.1 M phosphate buffer, 98%

• Empirische Formel (Hill-System): C₉H₁₂O₄
• CAS-Nummer: 139013-57-3
• Molekulargewicht: 184.19
• MDL-Nummer: MFCD01863551
• UNSPSC-Code: 12352103

Eigenschaften

• Assay: 98%
• Konzentration: 0.2 g/mL in 0.1 M phosphate buffer
• pH-Wert: 8.5(adjusted to)
• SMILES String: CC1(C)O[C@H]2[C@H](O)C=CC(=O)[C@H]2O1

Beschreibung

Physikalische Form

A suspension in phosphate buffer.

Rekonstituierung

To recover the pure product from the suspension:
(1)Thaw the frozen suspension and filter the solid. (2) Rinse bottle with a few milliliters of base-washed (aqueous Na₂CO₃) ethyl acetate. (3) Use the rinsing to wash the solid. (4) Collect solid. (5) To further collect more product from the filtrate: extract filtratewith equal volumes of base-washed (aqueous Na₂CO₃) ethyl acetate (repeat three times). (6) Dry the ethyl acetate extract over MgSO₄. (7) Evaporate the solvent - DO NOT HEAT! (8) Combine solids collected from the suspension and the filtrate. Pure crystals should be stored at -78° C. A suspension of the product in phosphate buffer is stable at 0° C.