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I7632

Sigma-Aldrich

Iodobenzene

98%

Synonyme(s) :

1-Iodobenzene, 4-Iodobenzene, Benzene iodide, Phenyl iodide

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5 G
54,30 $
100 G
94,00 $
500 G
373,00 $

About This Item

Formule empirique (notation de Hill) :
C6H5I
Numéro CAS:
591-50-4
Poids moléculaire :
204.01
Beilstein:
1446140
Numéro CE :
209-719-6
Numéro MDL:
MFCD00001029
Code UNSPSC :
12352100
ID de substance PubChem :
24896121
Nomenclature NACRES :
NA.22

54,30 $

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Essai

98%

Indice de réfraction

n20/D 1.62 (lit.)

pb

188 °C (lit.)

Pf

−29 °C (lit.)

Densité

1.823 g/mL at 25 °C (lit.)

Chaîne SMILES 

Ic1ccccc1

InChI

1S/C6H5I/c7-6-4-2-1-3-5-6/h1-5H

Clé InChI

SNHMUERNLJLMHN-UHFFFAOYSA-N

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Catégories apparentées

Description générale

Iodobenzene, also known as phenyl iodide, is commonly used as an arylating agent in various cross-coupling reactions.[1][2][3]

Application

Iodobenzene is used in various C-C coupling reactions.[4][5][6] It can be used in the preparation of iodobenzene dichloride, which is employed as an oxidant to oxidize alcohols to carbonyl compounds[7] and as a chlorinating agent.[8]

Pictogrammes

Exclamation mark
GHS07

Mention d'avertissement

Warning

Mentions de danger

H302

Classification des risques

Acute Tox. 4 Oral

Code de la classe de stockage

10 - Combustible liquids

Classe de danger pour l'eau (WGK)

WGK 3

Point d'éclair (°F)

170.6 °F - closed cup

Point d'éclair (°C)

77 °C - closed cup

Équipement de protection individuelle

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter

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Certificats d'analyse (COA)

Lot/Batch Number
BCCM7399
BCCL9575
BCCL1457
BCCJ3240
BCCF2534

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Consulter la Bibliothèque de documents

Iodobenzene dichloride as a stoichiometric oxidant for the conversion of alcohols into carbonyl compounds; two facile methods for its preparation.
Zhao, Xue-Fei and Zhang, Chi
Synthesis, 2007(04), 551-557 (2007)
Size effects of PVP- Pd nanoparticles on the catalytic Suzuki reactions in aqueous solution.
Li, Yin et al.
Langmuir, 18(12), 4921-4925 (2002)
Ring-Opening 1, 3-Dichlorination of Donor-Acceptor Cyclopropanes by Iodobenzene Dichloride.
Garve, Lennart KB et al.
Organic Letters, 16(21), 5804-5807 (2014)
Heck reactions of iodobenzene and methyl acrylate with conventional supported palladium catalysts in the presence of organic and/and inorganic bases without ligands.
Zhao, Fengyu et al.
Chemistry?A European Journal , 6(5), 843-848 (2000)
Thomas E Storr et al.
The Journal of organic chemistry, 74(16), 5810-5821 (2009-07-28)
Pd/Cu-mediated direct arylation of 2'-deoxyadenosine with various aryl iodides provides 8-arylated 2'-deoxyadenosine derivatives in good yields. Following significant reaction optimization, it has been determined that a substoichiometric quantity of piperidine (secondary amine) in combination with cesium carbonate is necessary for
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    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

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  2. How is shipping temperature determined? And how is it related to the product storage temperature?

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    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

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