Improved synthesis of chalcones under ultrasound irradiation.

Improved synthesis of chalcones under ultrasound irradiation.

Ultrasonics sonochemistry (2002-10-10)

Ji-Tai Li, Wen-Zhi Yang, Shu-Xiang Wang, Sheng-Hui Li, Tong-Shuang Li

RESUMO

Claisen-Schmidt condensation of acetophenone with aromatic aldehydes catalyzed by pulverized KOH and KF-Al2O3 results chalcones in 52-97% and 83-98% yields respectively in alcoholic solvent under ultrasound irradiation.

MATERIAIS

Número do produto

Marca

Descrição do produto

221473

Sigma-Aldrich

Hidróxido de potássio, ACS reagent, ≥85%, pellets

484016

Sigma-Aldrich

Hidróxido de potássio, reagent grade, 90%, flakes

306568

Sigma-Aldrich

Hidróxido de potássio, semiconductor grade, pellets, 99.99% trace metals basis (Purity excludes sodium content.)

06103

Sigma-Aldrich

Hidróxido de potássio, technical, ≥85%, powder

06005

Sigma-Aldrich

Hidróxido de potássio, puriss., meets analytical specification of Ph. Eur., BP, 85-100.5%, pellets

30603

Sigma-Aldrich

Hidróxido de potássio, pellets, reag. Ph. Eur., ≥85%

60370

Sigma-Aldrich

Hidróxido de potássio, puriss. p.a., ≥86% (T), pellets

911062

Sigma-Aldrich

Hidróxido de potássio, free-flowing, Redi-Dri^™, ACS reagent, ≥85%, pellets