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Merck

Rhodium-catalyzed [2 + 2] cycloaddition of ynamides with nitroalkenes.

Organic letters (2012-09-08)
Donna L Smith, Suresh Reddy Chidipudi, William R Goundry, Hon Wai Lam
RESUMO

In the presence of a diene-ligated rhodium complex, ynamides and nitroalkenes undergo catalytic [2 + 2] cycloadditions to provide cyclobutenamides. The presence of sodium tetraphenylborate was found to be crucial for the reactions to proceed efficiently.

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Sigma-Aldrich
Sodium tetraphenylborate, ACS reagent, ≥99.5%
Sigma-Aldrich
Potassium tetraphenylborate, 97%
Sigma-Aldrich
Ammonium tetraphenylborate, 99%
Sigma-Aldrich
Sodium tetraphenylborate, puriss. p.a., ACS reagent, ≥99.5% (NT)