GC Analysis of Total Petroleum Hydrocarbons (TPH) on SLB^®-5ms

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

45 °C (3 min), 20 °C/min to 360 °C (10 min)

inj. temp.

275 °C

detector

FID, 365 °C

carrier gas

helium, 1.3 mL/min. constant

injection

1.0 μL, 100:1 split

liner

2 mm I.D. straight

sample

TPH Mix 3, each analyte at 1000 μg/mL in carbon disulfide (861394-U)