Restlösemittel in pharmazeutischen Preparaten
Materialien
SPME-Faser
Produkt-Nr.
Beschreibung
Preisangaben
SPME-Faseranordnung Polydimethylsiloxan (PDMS)
df 100 μm(PDMS, needle size 24 ga, for use with manual holderCONDITIONS
SPME fiber
polydimethylsiloxane, 100 μm (57300-U)
extraction
headspace or immersion sampling (15 min) 1 min desorption
column
SPB-624, 75 m × 0.53 mm I.D., 3.0 μm (25432)
oven
40 °C (35 min) to 220 °C at 40 °C/min, hold 5 min
inj. temp.
splitless (closed 3 min), 200 °C
detector
FID, 250 °C
carrier gas
helium, 35 cm/sec
Beschreibung
Rechtliche Hinweise
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany