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G005580

GC Analysis of Sicilian Mandarin Essential Oil on SLB®-5ms

suitable for GC

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technique(s)

gas chromatography (GC): suitable

test parameters

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 50 °C, 3 °C/min. to 250 °C (10 min), 10 °C/min to 270 °C (3 min)
inj. temp.: 280 °C
detector: FID, 280 °C
carrier gas: helium, 30 cm/sec, constant
injection: 1 μL, 50:1 split
sample: Sicilian mandarin essential oil diluted 1:10 in n-hexane

application(s)

flavors and fragrances

Analysis Note

Sicilian mandarin essential oil, which is derived by cold pressing of the peel of Citrus deliciosa, is used in both food and cosmetic preparations for its desirable fragrance and flavoring properties. This application demonstrates the analysis of this material on the SLB-5ms. The separation illustrates the complexity of this essential oil, which consists of volatile, non-volatile, and chiral components.

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

analytical column

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