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97-0189

GC Analysis of a 7-Component Sulfur Gases Mix on Supel-Q PLOT after SPME using 75 μm Carboxen/PDMS Fiber

suitable for GC, application for SPME

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technique(s)

gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable

test parameters

sample/matrix: sulfur gases in 40 mL vial
SPME fiber: Carboxen/PDMS, 75 μm (57318)
extraction: 10 min headspace at 40 °C
desorption process: 3 min at 290 °C
column: Supel-Q PLOT, 30 m × 0.32 mm I.D. (24242)
oven: 45 °C (1 min) to 250 °C at 15 °C/min
detector: FPD

suitability

application for SPME

application(s)

chemicals and industrial polymers

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Description

    Sulfur dioxide
    Hydrogen sulfide
    Carbonyl sulfide
    Methanethiol
    Ethanethiol
    Dimethyl disulfide
    Carbon disulfide

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