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Key Documents

1.88054

Supelco

Water Standard

1%, Certified Reference Material for KF oven method Aquastar®

Synonym(s):

TM=["AQUASTAR"] Water Standard Oven 1% for KF oven method

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5 G
$185.00

$185.00


Estimated to ship onJuly 04, 2025


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5 G
$185.00

About This Item

UNSPSC Code:
41115601
NACRES:
NA.24

$185.00


Estimated to ship onJuly 04, 2025


Request a Bulk Order

Product Name

Water Standard Oven 1%, Certified Reference Material for KF oven method Aquastar®

grade

certified reference material

Quality Level

agency

ISO 17025, 17034

product line

Aquastar®

form

solid

technique(s)

Karl-Fischer titration: suitable
titration: suitable

bulk density

460 kg/m3

format

neat

storage temp.

15-25°C

General description

It is a solid standard prepared gravimetrically from high-purity reagents. The water content of it is determined by coulometric Karl Fischer oven method at 170°C with an extraction time of 600 seconds following ISO 760. Additionally, its measured water content is verified by thermogravimetric analysis. Unlike other solid standards such as tartrate, lactose, or citrate, the water standard oven 1% has significantly lower water content and can be used over a broad temperature range of 150°C to 400°C due to its inorganic composition. It is characterized in accredited quality control (QC) laboratory according to DIN EN ISO/IEC 17025.
Please visit ISO certificates and Site Quality Self-Assessments to access the current certificates of accreditation.
Download your certificate at http://www.sigma-aldrich.com to view certified values, including uncertainty and expiry date.

Application

Water standard oven 1% is used as certified reference material to check the accuracy of coulometric and volumetric water determinations, according to ISO 9001 chapter 7.1.5 “Monitoring and measuring resources”, using Karl Fischer oven and thermobalances. But its low water content of 1% makes it particularly suitable for water determinations using Karl Fischer oven with a coulometer.

Features and Benefits

  • Packed in convenient glass bottles with the material subjected to stability and homogeneity studies following ISO 17034 and ISO Guide 35
  • Supplied with a batch-specific certificate of analysis (CoA) having data on exact measured water, uncertainty, method of analysis, measuring method, and minimum shelf life
  • Characterized in an ISO/IEC 17025 and ISO 17034 accredited calibration laboratory
  • Directly traceable to SI unit (kg)

Linkage

Replaces: 1.88054.0005

Legal Information

AQUASTAR is a registered trademark of Merck KGaA, Darmstadt, Germany

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Storage Class

13 - Non Combustible Solids

wgk_germany

WGK 2

flash_point_f

Not applicable

flash_point_c

Not applicable


Certificates of Analysis (COA)

Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.

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Questions

1–4 of 4 Questions  
  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

      Helpful?

  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Helpful?

  3. What should be done if Water Standard Oven 1% experiences a decrease in water content when stored under argon in a glove box?

    1 answer
    1. It is not recommended to store the 1% water standard oven in a glove box. Storing it in environments with low humidity can cause a decrease in its water content. To maintain the standard's integrity, it is crucial to tightly seal the bottles immediately after use and store them under normal laboratory or environmental conditions.

      Helpful?

  4. buenos dias, a que temperatura esta certificado este std ?

    1 answer
    1. As cited in the product Certificate of Analysis, the water content is determined by the coulometric Karl Fischer oven method at 170°C".

      TS Answer: Product 1.88054 (which may also be written without the dot as 188054) is a water standard composed of a mixture of potassium sulfate and sodium tungsten dihydrate, provided as a powder. It is approximately 1 percent water by weight or 10 milligrams of water per 1 gram of powder; the exact certified value as a mass fraction or mass percentage is reported on the certificate of analysis (CofA) for each lot.

      This standard is to be stored at room temperature (15-25°C), up to the lot-specific expiry date. But the analysis is run at a much higher temperature. The Measurement method provided on the Certificate of Analysis says "The water content is determined by coulometric Karl Fischer oven method at 170°C".

      Helpful?

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