Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf
1.06044
Dichloromethane
for liquid chromatography LiChrosolv®
Synonym(s):
DCM, Methylene chloride, Methylene dichloride, Methylene chloride
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About This Item
6.83 psi ( 20 °C)
Recommended Products
vapor density
2.9 (vs air)
Quality Level
vapor pressure
24.45 psi ( 55 °C)
6.83 psi ( 20 °C)
product line
LiChrosolv®
grade
isocratic
assay
≥99.9% (GC)
form
liquid
autoignition temp.
1223 °F
605 °C (DIN 51794)
potency
1600 mg/kg LD50, oral (Rat)
>2000 mg/kg LD50, skin (Rat)
contains
2-methyl-2-butene as stabilizer
expl. lim.
22 %
technique(s)
HPLC: suitable
impurities
≤0.0002 meq/g Acidity
≤0.0002 meq/g Alkalinity
≤0.01% Water
evapn. residue
≤5.0 mg/L
transmittance
240 nm, ≥70%
245 nm, ≥90%
260 nm, ≥99%
refractive index
n20/D 1.424 (lit.)
pH
7 (20 °C)
bp
39.8-40 °C (lit.)
mp
-95 °C
−95 °C (lit.)
solubility
20 g/L
density
1.325 g/mL at 25 °C (lit.)
storage temp.
2-30°C
SMILES string
ClCCl
InChI
1S/CH2Cl2/c2-1-3/h1H2
InChI key
YMWUJEATGCHHMB-UHFFFAOYSA-N
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General description
Application
Features and Benefits
- suitability tested and specified for UHPLC-MS and UHPLC-UV: for analytical flexibility
- specified quality in positive and negative in positive and negative electrospray ionization (ESI) and atmospheric-pressure chemical ionization-mass spectrometry (APCI-MS) for lowest detection limits and confidence in analyses for all important MS modes (test 1)
—ESI/APCI (+) < 2 ppb
—ESI/APCI (-) < 10 ppb - lowest impurity profile: for interference-free baselines (test 2)
- microfiltered through 0.2 μm filter (test 3) to provide:
—a long lifespan to filters and mechanical parts of HPLC systems
—reduced risk of column clogging - packed in borosilicate glass bottles for minimum metal ion contaminations
- lowest levels of trace metal impurities for a minimum metal ion adduct formation
—< 5ppb - lowest level of polyethylene glycol (PEG) impurities in UHPLC-MS solvent lineup (PEG S/N signal-to-noise-ratio < 50)
Preparation Note
Analysis Note
Identity (IR): conforms
Acidity: ≤ 0.0002 meq/g
Alkalinity: ≤ 0.0002 meq/g
Transmission (at 240 nm): ≥ 70 %
Transmission (at 245 nm): ≥ 90 %
Transmission (from 260 nm): ≥ 99 %
Evaporation residue: ≤ 5.0 mg/l
Water: ≤ 0.01 %
The product is stabilized with 2-Methyl-2-buten.
Filtered by 0.2 µm filter
Other Notes
Legal Information
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signalword
Warning
hcodes
Hazard Classifications
Carc. 2 - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Central nervous system
Storage Class
6.1D - Non-combustible acute toxic Cat.3 / toxic hazardous materials or hazardous materials causing chronic effects
wgk_germany
WGK 2
flash_point_f
does not flash
flash_point_c
does not flash
Certificates of Analysis (COA)
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How is shipping temperature determined? And how is it related to the product storage temperature?
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If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdfHelpful?
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