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417475

Sigma-Aldrich

6-Methylchromone hydrate

98%

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About This Item

Empirical Formula (Hill Notation):
C10H8O2 · xH2O
CAS Number:
Molecular Weight:
160.17 (anhydrous basis)
MDL number:
UNSPSC Code:
12352100
PubChem Substance ID:
NACRES:
NA.22

assay

98%

form

solid

mp

76-78 °C (lit.)

SMILES string

[H]O[H].Cc1ccc2OC=CC(=O)c2c1

InChI

1S/C10H8O2.H2O/c1-7-2-3-10-8(6-7)9(11)4-5-12-10;/h2-6H,1H3;1H2

InChI key

QWIQUUMSUBFRAX-UHFFFAOYSA-N

General description

6-Methylchromone hydrate is a chromone derivative. Chromones are cyclic compounds containing nine carbon atoms with sp2 hybridization. They are commonly referred as 1,4-benzapyranes or γ-benzopyrones.

Application

6-Methylchromone may be employed as activated alkene in the methanolic trimethylamine or sodium methoxide catalyzed Baylis-Hillman coupling reaction with aromatic and aliphatic aldehydes.

pictograms

Exclamation mark

signalword

Warning

hcodes

Hazard Classifications

Acute Tox. 4 Oral

Storage Class

11 - Combustible Solids

wgk_germany

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable


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Vyacheslav Ya Sosnovskikh et al.
The Journal of organic chemistry, 71(12), 4538-4543 (2006-06-06)
Polyhaloalkyl-substituted chromones, gamma-pyrones, and beta-furanones react with salicylaldehydes in the presence of piperidine to give a wide variety of fused 2H-chromenes in good yields. This novel annulation reaction presumably proceeds by a tandem intermolecular oxa-Michael addition and subsequent intramolecular Mannich
The standard molar enthalpies of formation of chromone-3-carboxylic acid, 6-methylchromone-2-carboxylic acid, and 6-methyl-4-chromanone determined by micro-combustion calorimetry.
Flores H, et al.
Journal of Thermal Analysis and Calorimetry, 117(1), 433-437 (2014)

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