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Merck

Pd-NHC catalyzed conjugate addition versus the Mizoroki-Heck reaction.

Chemistry (Weinheim an der Bergstrasse, Germany) (2011-02-10)
Aditya L Gottumukkala, Johannes G de Vries, Adriaan J Minnaard
摘要

Ace of base: A catalytic system is presented that, solely by choice of the base, selectively switches between conjugate addition and the Mizoroki-Heck reaction of aryl halides with Michael acceptors (see scheme; R, R' = alkyl, aryl). For conjugate addition reactions, this avoids the preparation and use of organometallics.

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Sigma-Aldrich
4-苯基-3-丁烯-2-酮, 99%
Sigma-Aldrich
亚苄基丙酮, ≥98%, FG
Sigma-Aldrich
特戊酸铯, 98%
Sigma-Aldrich
反式-4-苯基-3-丁烯-2-酮, ≥99%