技術
gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable
測試參數
sample/matrix: 200 ppt each in 2 mL water
SPME fiber: polydimethylsiloxane, 100 μm (57300-U)
extraction: 15 min immersed in water with rapid stirring
column: SPB-5, 15 m × 0.20 mm I.D., 0.20 μm (24165-U)
oven: 120 °C (1 min) to 180 °C at 30 °C/min, then to 290 °C at 10 °C/min
inj. temp.: 260 °C (splitless - closed 3 min)
detector: ECD, 300 °C
carrier gas: helium, 37 cm/sec (set at 120 °C)
適合性
application for SPME
應用
environmental
food and beverages
法律資訊
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
描述
4,4′-DDD, PESTANAL®, analytical standard
Endrin aldehyde
Aldrin
Dieldrin
α-BHC
Endosulfan sulfate
Endrin ketone
α-Chlordane
γ-Chlordane
δ-BHC
Decachlorobiphenyl
4,4′-DDT
Methoxychlor
Heptachlor
γ-BHC, certified reference material, 1000 μg/mL in methanol
Endrin
β-BHC
1,1-Dichloro-2,2-bis(4-chlorophenyl)ethene
Heptachlor epoxide, PESTANAL®, analytical standard, isomer B
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