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Merck
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33040-U

Supelco

三氟化硼-甲醇

10 % (w/w)

同義詞:

三氟化硼

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About This Item

分類程式碼代碼:
12000000

等級

for GC derivatization

反應適用性

reagent type: derivatization reagent
reaction type: Alkylations

reagent type: derivatization reagent
reaction type: Esterifications

包裝

pkg of 10 × 5 mL

濃度

10 % (w/w)

儲存溫度

2-8°C

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一般說明

Boron trifluoride is a colourless gas and it reacts readily with water to form hydrates. It has been widely used as a catalyst during polymerizations, alkylations and condensation reactions. It is used as gas flux for internal soldering or brazing. It also finds application in being used as extinguisher for magnesium fires.

應用

It was used in transmethylation of 1,2-Diacylglycerol (DAG) containing fractions which were purified using HPLC. It may be used to treat lipids during GC analysis done for determination of fatty acid methyl esters and dimethylacetals.

其他說明

Reagent for O-acetyl, methyl ester, methyl 2,2-dimethoxypropionate, dimethyl acetals and dimethoxy.

訊號詞

Danger

危險分類

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1A - STOT RE 2 Inhalation - STOT SE 1

標靶器官

Eyes, Kidney

儲存類別代碼

3 - Flammable liquids

水污染物質分類(WGK)

WGK 2

閃點(°F)

60.8 °F - closed cup

閃點(°C)

16 °C - closed cup

個人防護裝備

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter


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分析證明 (COA)

Lot/Batch Number

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存取文件庫

D.R. Knapp
Handbook of Analytical Derivatization Reactions, 438-438 (1979)
S B Bocckino et al.
The Journal of biological chemistry, 260(26), 14201-14207 (1985-11-15)
1,2-Diacylglycerol (DAG) was measured in neutral lipid extracts from isolated hepatocytes using high pressure liquid chromatography followed by refractive index detection. Maximally effective doses of epinephrine, angiotensin II, and vasopressin increased DAG by approximately 65, 80, and 180-250%, respectively, with
PREPARATION OF FATTY ACID METHYL ESTERS AND DIMETHYLACETALS FROM LIPIDS WITH BORON FLUORIDE--METHANOL.
W R MORRISON et al.
Journal of lipid research, 5, 600-608 (1964-10-01)
ANALYSIS OF HYDROXY FATTY ACIDS BY GAS-LIQUID CHROMATOGRAPHY.
J S O'BRIEN et al.
Analytical biochemistry, 7, 288-296 (1964-03-01)
Compressed Gas Association
Handbook of Compressed Gases, 271-271 (2012)

條款

Analyze omega 3 fatty acid profiles from fish oil capsules and salmon using GC columns for confirmatory analysis of lipid composition.

使用 GC 色譜柱分析來自魚油膠囊和鮭魚的奧米加 3 脂肪酸,以確認脂質組成的分析。

Chromatograms

suitable for GC, application for SPEsuitable for GCsuitable for GCsuitable for GC, application for SPE顯示更多

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