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Merck
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重要文件

21006

Supelco

Apiezon® L

phase Apiezon L, bottle of 25 g

同義詞:

GC 固定相

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About This Item

分類程式碼代碼:
41115717

形狀

solid

包裝

bottle of 25 g

參數

50-300 °C temp. range

技術

gas chromatography (GC): suitable

基質活性組

Apiezon L phase

溶解度

chloroform, toluene: soluble

柱類型

packed GC

一般說明

合成的产品更纯净,分子量范围窄,不含用作 GC 固定相的痕量催化剂或杂质。
GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation and peak tailing are a few parameters which are considered while choosing a stationary phase. Apiezon L is basically purified hydrocarbon grease which is suitable as a liquid phase for GC analysis. It is considered as one of the most selective phase for Polychlorinated Biphenyls (PCB) congeners.

應用

Apiezon L may be used as stationary phase to determine the retention indices of benzene and benzene derivatives on the basis of their molecular structure using GC equipped with a thermal conductivity detector.

儲存類別代碼

13 - Non Combustible Solids

水污染物質分類(WGK)

WGK 3

閃點(°F)

Not applicable

閃點(°C)

Not applicable

個人防護裝備

Eyeshields, Gloves, type N95 (US)


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分析證明 (COA)

Lot/Batch Number

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Calculation of retention indices for benzene and benzene derivatives on the basis of molecular structure.
Cook, Lawrence E., and Frank M. Raushel.
Journal of Chromatography A, 65, 556-559 (1972)
Mitchell D. Erickson
Analytical Chemistry of PCBs, 250-250 (1997)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)

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