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Merck

73120

Supelco

4-硝基苯甲酰氯

for HPLC derivatization, LiChropur, ≥99.0% (GC)

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100 G
$160.00

About This Item

线性分子式:
O2NC6H4COCl
CAS号:
分子量:
185.56
Beilstein:
473192
EC號碼:
MDL號碼:
分類程式碼代碼:
12000000
PubChem物質ID:
NACRES:
NA.22

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等級

for HPLC derivatization

品質等級

化驗

≥99.0% (GC)

形狀

crystals

品質

LiChropur

技術

HPLC: suitable

燃燒殘留物

≤0.05% (as SO4)

bp

202-205 °C/105 mmHg (lit.)

mp

71-74 °C (lit.)
71-74 °C

SMILES 字串

[O-][N+](=O)c1ccc(cc1)C(Cl)=O

InChI

1S/C7H4ClNO3/c8-7(10)5-1-3-6(4-2-5)9(11)12/h1-4H

InChI 密鑰

SKDHHIUENRGTHK-UHFFFAOYSA-N

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一般說明

4-Nitrobenzoyl chloride is a derivatization reagent. It reacts with L-glutamic acid undergoing methylation using formaldehyde, synthesizing N-(4-methylaminobenzoyl)glutaminic acid.[1]

應用

4-Nitrobenzoyl chloride was used in separating polyhydric alcohols using HPLC.[2] It was used in snythesizing cellulose benzotates by adding to cellulose/1-allyl-3-methylimidazolium chloride followed by characterization using FT-IF, 1H-NMR and 13C-NMR spectroscopy.[3] It may be used in synthesizing 1-aryloxyacetyl-4-(4-nitrobenzoyl)-thiosemicarbazides under phase transfer catalysis and microwave irradiation with ammonium thiocyanate and aryloxyacetic acid hydrazides.[4]

其他說明

HPLC 羟基衍生化[5][6]

推薦產品

Discover LiChropur reagents ideal for HPLC or LC-MS analysis

法律資訊

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

象形圖

Corrosion

訊號詞

Danger

危險聲明

危險分類

Eye Dam. 1 - Met. Corr. 1 - Skin Corr. 1B

儲存類別代碼

8A - Combustible corrosive hazardous materials

水污染物質分類(WGK)

WGK 1

閃點(°F)

215.6 °F - closed cup

閃點(°C)

102 °C - closed cup

個人防護裝備

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges


历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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其他客户在看

Slide 1 of 2

1 of 2

The synthesis of silica-immobilized 1, 2-naphthoquinone thiosemicarbazone with 3-aminopropyltriethoxy silane and 4-nitrobenzoyl chloride.
Audu, Aramani A.
Reactive Polymers, 10, 3-9 (1989)
F Nachtmann et al.
Journal of chromatography, 122, 293-303 (1976-07-07)
The separation and quantitative determination of digitalis glycosides by high performance liquid chromatography following derivatization with 4-nitrobenzoylchloride (4-NBC1) is described. The compounds of primary interest were the digitalis glycosides and aglycones of the pharmaceutically important A, B and C series
Ruben Vardanyan, Victor Hruby
Synthesis of Essential Drugs, 391-391 (2006)
Journal of Chromatography A, 136, 279-279 (1977)
Separation of some polyhydric alcohols by high-performance liquid chromatography.
Schwarzenbach, Rolf.
Journal of Chromatography A, 140, 304-309 (1977)

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