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Merck
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368873

Sigma-Aldrich

9-溴-9-苯基芴

97%

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About This Item

经验公式（希尔记法）:
C19H13Br
CAS号:
55135-66-5
分子量:
321.21
MDL编号:
MFCD00075522
UNSPSC代码:
12352100
PubChem化学物质编号:
24862938
NACRES:
NA.22

方案

97%

mp

99-101 °C (lit.)

官能团

bromo
phenyl

SMILES字符串

BrC2(c1ccccc1)c3ccccc3-c4ccccc24

InChI

1S/C19H13Br/c20-19(14-8-2-1-3-9-14)17-12-6-4-10-15(17)16-11-5-7-13-18(16)19/h1-13H

InChI key

HYQXNCDBSALQLB-UHFFFAOYSA-N

一般描述

Solvolysis of 9-bromo-9- phenylfluorene has been reported to proceed via limiting SN1 mechanism.[1]

应用

9-Bromo-9-phenylfluorene may be used in the preparation of:
  • N-(9-(9-phenylfluorenyl))-L-alaninal[2]
  • N-(9-phenylfluoren-9-yl)-L-serine[3]
  • 1-hydroxypyrazoles priotected at the oxygen atom[4]

象形图

Corrosion
GHS05

警示用语：

Danger

危险声明

H314

危险分类

Eye Dam. 1 - Skin Corr. 1B

储存分类代码

8A - Combustible corrosive hazardous materials

WGK

WGK 3

闪点(°F)

Not applicable

闪点(°C)

Not applicable

个人防护装备

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges

历史批次信息供参考:

分析证书(COA)

Lot/Batch Number
0000083805
0000071401
03907CJ
07223LD
06412KD

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Surrogates for Chiral Aminomalondialdehyde. Synthesis of N-(9-Phenylfluoren-9-yl) serinal and N-(9-Phenylfluoren-9-yl) vinylglycinal.
Lubell WD and Rapoport H.
The Journal of Organic Chemistry, 54(16), 3824-3831 (1989)
Configurational stability of N-protected. alpha.-amino aldehydes.
Lubell WD and Rapoport H.
Journal of the American Chemical Society, 109(1), 236-239 (1987)
Synthesis of 5-substituted 1-hydroxypyrazoles through directed lithiation of 1-(benzyloxy) pyrazole.
Vedso P and Begtrup M.
The Journal of Organic Chemistry, 60(16), 4995-4998 (1995)
Solvent and Substituent Effects in the Solvolysis of 9-Aryl-9-bromofluorenes.
Liu K-T and Lin Y-S.
J. Chin. Chem. Soc., 47(1), 71-76 (2000)

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