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Merck

15256

Supelco

BSA+TMCS

for GC derivatization, LiChropur, 93.0-97.0% (GC)

Sinónimos:

Bis(trimethylsilyl)acetamide + Trimethylchlorosilane

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About This Item

Código UNSPSC:
41116105
ID de la sustancia en PubChem:
NACRES:
NA.22

grado

for GC derivatization

Nivel de calidad

Ensayo

93.0-97.0% (GC)

calidad

LiChropur

composición

trimethylchlorosilane (minor component), 3.0-5.0% GC

idoneidad de la reacción

reagent type: derivatization reagent
reaction type: Silylations

técnicas

gas chromatography (GC): suitable

Descripción general

BSA+TMCS combination, is one of the most commonly used silylating reagents. BSA is readily used for silylating a wide range of functional groups such as non-sterically hindered alcohols, amides, amines, amino acids, carboxylic acids, and enols. TMCS is a silylation catalyst always used with other silylation reagents to increase the reactivity in derivatization of alcohols, alkaloids, amines, biogenic amines, carboxylic acids, phenols, and steroids.

Aplicación

Learn more in the Product Information
Suitable for the derivatization of α-ketoacids, amines, amino acids, cycloserine, histamine and metabolites, phenylethylamines, phosphatidylserines and tryptamines. BSA+TMCS may be used as a derivatizing reagent for the determination of steryl glycosides in biodiesel using gas chromatography–mass spectrometry.
Suitable for the derivatization of a-ketoacids, amines, amino acids, cycloserine, histamine and metabolites, phenylethylamines, phosphatidylserines and tryptamines.

Características y beneficios

  • BSA+TMCS has good solvent properties and can function as a silylation reagent without additional solvents.        
  • Alternatively, the mixture is very soluble in most commonly used silylation solvents.        
  • This combination is extremely sensitive to moisture and should be handled under dry conditions.

Otras notas

Poderosa mezcla de sililación para amplio número de aplicaciones
Reagent for trimethylsilyl diglyceride, trimethylsilyl (TMS) and trimethylsilyl oximes.

Información legal

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

Producto relacionado

Referencia del producto
Descripción
Precios

Palabra de señalización

Danger

Frases de peligro

Clasificaciones de peligro

Acute Tox. 4 Oral - Flam. Liq. 2 - Skin Corr. 1A

Riesgos supl.

Código de clase de almacenamiento

3 - Flammable liquids

Clase de riesgo para el agua (WGK)

WGK 3

Punto de inflamabilidad (°F)

53.6 °F - closed cup

Punto de inflamabilidad (°C)

12 °C - closed cup

Equipo de protección personal

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter


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P. Englmaier
Z. Anal. Chem., 324, 338-338 (1986)
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Frontiers in neurology, 10, 1157-1157 (2019-11-19)
Background and objective: Chronic relapsing inflammatory optic neuritis (CRION) is one of the more common phenotypes related to myelin oligodendrocyte glycoprotein antibodies (MOG-Abs). The absence of specific biomarkers makes distinguishing between CRION and relapsing inflammatory ON (RION) difficult. A recent
Removal of pharmaceuticals during drinking water treatment.
Terness TA
Environmental Science & Technology, 36 (17), 3855-3863 (2002)
D.L. Sondack et al.
Journal of Pharmacological Sciences, 62, 1344-1344 (1973)
D.R. Knapp
Handbook of Analytical Derivatization Reactions, 202-202 (1979)

Artículos

Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs

Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs

Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs

Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs

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