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260908

Sigma-Aldrich

N-Bromophthalimide

95%

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25 G
€158.00

€158.00

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25 G
€158.00

About This Item

Empirical Formula (Hill Notation):
C8H4BrNO2
CAS Number:
2439-85-2
Molecular Weight:
226.03
Beilstein:
131211
EC Number:
219-467-9
MDL number:
MFCD00005888
UNSPSC Code:
12352100
PubChem Substance ID:
24855777
NACRES:
NA.22

€158.00

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Quality Level

100

Assay

95%

mp

194-198 °C (lit.)

functional group

imide

SMILES string

BrN1C(=O)c2ccccc2C1=O

InChI

1S/C8H4BrNO2/c9-10-7(11)5-3-1-2-4-6(5)8(10)12/h1-4H

InChI key

MARXMDRWROUXMD-UHFFFAOYSA-N

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Application

N-Bromophthalimide has been used:
  • as reagent in allylic amination reactions of alkenes[1]
  • brominating reagent in enantioselective synthesis of multisubstituted biaryl derivatives by chiral phosphoric acid catalyzed asymmetric bromination[2]
  • as a titrant in titrimetric determination of isoniazid in pure form or in tablets[3]

Pictograms

Exclamation mark
GHS07

Signal Word

Warning

Hazard Statements

H315,H319,H335

Hazard Classifications

Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

Target Organs

Respiratory system

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

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Certificates of Analysis (COA)

Lot/Batch Number
STBK0193
STBJ4191
STBH3040
STBF4285V
STBD9654V

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Titrimetric determination of para-aminobenzoic acid using N-bromophthalimide and N-bromosaccharin.
K G Kumar et al.
Journal of pharmaceutical and biomedical analysis, 7(5), 627-631 (1989-01-01)
Titrimetric methods for the determination of some sulpha drugs using N-bromophthalimide and N-bromosaccharin.
K G Kumar et al.
The Analyst, 113(9), 1369-1372 (1988-09-01)
Tejas P Pathak et al.
Journal of the American Chemical Society, 134(14), 6120-6123 (2012-04-03)
We report the site-selective bromination of vancomycin to produce, with substantial efficiency, previously unknown monobromovancomycins, a dibromovancomycin, and a tribromovancomycin. We document the inherent reactivity of native vancomycin toward N-bromophthalimide. We then demonstrate significant rate acceleration and perturbation of the
A M el-Brashy et al.
Journal of pharmaceutical and biomedical analysis, 10(6), 421-426 (1992-06-01)
Two methods are proposed for the determination of isoniazid in pure form or in tablets. In the first method chlorpromazine hydrochloride, when treated with 2-iodoxybenzoic acid as an oxidant in 50% w/v o-phosphoric acid solution, is oxidized to chlorpromazine free
V Krishnakumar et al.
Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 62(4-5), 918-925 (2005-06-14)
Fourier transform infrared (FT-IR) spectra of phthalimide and N-bromophthalimide have been recorded in the range of 4000-400 cm-1. With the hope of providing more and effective information on the fundamental vibrations, a normal coordinate analysis has been performed on phthalimide
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