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28471-U

Supelco

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Synonym(s):

GC column, SPB-5, 5% diphenyl, mass spec

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About This Item

UNSPSC Code:
12000000
eCl@ss:
32119290
NACRES:
SB.54
Pricing and availability is not currently available.

material

fused silica

Quality Level

Agency

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

reg. compliance

FDA LIB 4423

parameter

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

Beta value

250

df

0.25 μm

technique(s)

GC/MS: suitable
gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

column type

capillary non-polar

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General description

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded and highly crosslinked
  • Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
  • ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Application


  • Determination of propargite, tebuconazole and bromopropylate pesticide residues in Taiwan green jujubes by gas chromatography-tandem mass spectrometry.: This study utilized the SLB-5ms Capillary GC Column to analyze pesticide residues in agricultural produce. The method demonstrated high sensitivity and specificity, highlighting the column′s efficacy in complex sample matrices (Zhang et al., 2014).

  • Characterisation of capillary ionic liquid columns for gas chromatography-mass spectrometry analysis of fatty acid methyl esters.: The research explored the performance of SLB-5ms Capillary GC Columns for the analysis of fatty acid methyl esters. The column exhibited superior resolution and stability, making it a valuable tool for lipid analysis in biochemical applications (Zeng et al., 2013).

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Tommy W McGaha et al.
PloS one, 10(3), e0118904-e0118904 (2015-03-19)
The suite of pheromones that promote communal oviposition by Simulium vittatum, a North American black fly species, was identified and characterized using gas chromatography-mass spectrometry, electrophysiological, and behavioral bioassays. Behavioral assays demonstrated that communal oviposition was induced by egg-derived compounds
Chemical Characterization of Three Accessions of Brassica juncea L. Extracts from Different Plant Tissues
Oulad El Majdoub Y, et al.
Molecules (Basel), 25(22), 5421-5421 (2020)
Lorenzo Cucinotta et al.
Journal of chromatography. A, 1655, 462473-462473 (2021-09-01)
The use of IRMS as a GC detector has a history going back decades, however the critical issue of wrong δ13C measurements resulting from impure peaks has been often underestimated. To this regard, multidimensional separation techniques are effective tools to
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction
Annie Xu Zeng et al.
Analytica chimica acta, 803, 166-173 (2013-11-13)
Due to their distinct chemical properties, the application of ionic liquid (IL) compounds as gas chromatography (GC) stationary phases offer unique GC separation especially in the analysis of geometric and positional fatty acid methyl ester (FAME) isomers. Elution behaviour of

Articles

GC Analysis of Neroli Essential Oil on SLB®-5ms

Resolving by Mass

Protocols

GC Analysis of PBDE Flame-Retardant Compounds

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

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Chromatograms

suitable for GCsuitable for GC, application for SPMEsuitable for GC, application for SPMEsuitable for GCShow More

Questions

1–6 of 6 Questions  
  1. How does the SLB™-5ms Capillary GC Column differ from our other 5-type columns?

    1 answer
    1. Many of our other 5-type columns (Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S) incorporate a siloxane polymer (backbone comprised of Si and O atoms only, side groups are either methyl or phenyl). The SLB-5ms column incorporates a silphenylene polymer (backbone comprised of Si and O atoms plus some phenyl groups, side groups are either methyl or phenyl).

      Helpful?

  2. Would you recommend SLB™-5ms Capillary GC Columns for all applications instead of Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S?

    1 answer
    1. Yes.

      Helpful?

  3. What is the Department of Transportation shipping information for this product?

    1 answer
    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

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  4. Who uses SLB™-5ms Capillary GC Columns?

    1 answer
    1. Any analyst with the need for a non-polar column. Some applications include boiling point separations, GC-MS analyses of semivolatiles, and GC-ECD analyses of pesticides/PCBs. It is estimated that non-polar columns account for 51% of the worldwide column market.

      Helpful?

  5. What are the benefits of the SLB™-5ms Capillary GC Column over other manufacturers’ -5ms columns?

    1 answer
    1. The SLB-5ms excels in several performance criteria.· Low Bleed. The highly crosslinked silphenylene polymer chemistry reduces column bleed to a very low level, resulting in greater signal-to-noise level, allowing lower detection levels.· Inertness. The proprietary surface deactivation reduces interactions between analytes and the column surface, resulting in sharper peak shapes, allowing lower detection levels.· Durability. With the highest published maximum allowable operating temperature (MAOT) of any -5ms column, SLB-5ms columns are designed for long life.· Consistency. Innovative manufacturing processes result in decreased column variability, ensuring that the next column is as good as the last.

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  6. What if my method does not allow me to change to SLB™-5ms Capillary GC Columns?

    1 answer
    1. These methods typically specify a 5-type column (DB-5 or equivalent). The SLB-5ms satisfies that requirement.

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