8.55026

4-Benzyloxybenzaldehyde polystyrene HL

Novabiochem^®

• 別名: Aldehyde Wang HL resin
• UNSPSCコード: 13111023
• NACRES: NA.22

特性

• 品質水準: 200
• 製品種目: Novabiochem^®
• 形状: beads
• 反応適合性: reaction type: Fmoc solid-phase peptide synthesis
• メーカー／製品名: Novabiochem^®
• アプリケーション: peptide synthesis
• 官能基: alcohol
• 保管温度: 2-8°C

詳細

詳細

This support is an excellent tool for the production of sulfonamides and anilides by SPOS ^[1]. Amines have been released from this resin with DDQ ^[2] and tertiary amides by acylation of resin-bound secondary amines with acid chlorides ^[3].

Associated Protocols and Technical Articles
Protocols for Loading of Peptide Synthesis Resins

Literature references

^[1] B. Raju & T. P. Kogan (1997) Tetrahedron Lett., 38, 4965.
^[2] S. Kobayashi & Y. Aoki (1998) Tetrahedron Lett., 39, 7345.
^[3] M. W. Miller, et al. (1998) Tetrahedron Lett., 39, 3429.

関連事項

Replaces: 01-64-0182

アナリシスノート

Color (visual): white to yellow to orange
Appearance of substance (visual): beads
Loading (determined by elemental analysis of sulfur after derivatization with tosylhydrazide): 2.0 - 3.5 mmol/g
Swelling Volume (in DMF): lot specific result
The polymer matrix is copoly(styrene - 2% DVB), 200 -400 mesh.

法的情報

Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany

安全性情報

• 保管分類コード: 11 - Combustible Solids
• WGK: WGK 1
• 引火点(°F): Not applicable
• 引火点(℃): Not applicable