8.53018

Boc-Lys(2-Cl-Z)-OH

(cryst) Novabiochem^®

• 別名: Boc-Lys(2-Cl-Z)-OH, N-α-t.-Boc-N-ε-2-chloro-CBZ-L-lysine
• 実験式（ヒル表記法）: C₁₉H₂₇ClN₂O₆
• CAS番号: 54613-99-9
• 分子量: 414.88
• MDL番号: MFCD00356585
• UNSPSCコード: 12352209
• NACRES: NA.22

特性

• 品質水準: 200
• 製品種目: Novabiochem^®
• アッセイ: ≥95.0% (acidimetric); ≥98% (TLC); ≥99.0% (HPLC)
• フォーム: powder
• 反応適合性: reaction type: Boc solid-phase peptide synthesis
• メーカー／製品名: Novabiochem^®
• mp: 70-73 °C
• アプリケーション: peptide synthesis
• 官能基: amine
• 保管温度: 2-8°C
• SMILES記法: Clc1c(cccc1)COC(=O)NCCCCC(NC(=O)OC(C)(C)C)C(=O)O
• InChI: 1S/C19H27ClN2O6/c1-19(2,3)28-18(26)22-15(16(23)24)10-6-7-11-21-17(25)27-12-13-8-4-5-9-14(13)20/h4-5,8-9,15H,6-7,10-12H2,1-3H3,(H,21,25)(H,22,26)(H,23,24)
• InChI Key: ATUMDPHEFWGCJF-UHFFFAOYSA-N

詳細

詳細

Standard building block for introduction of lysine amino-acid residues by Boc SPPS.

Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS

Literature references

^[1] K. Noda, et al. (1969) Bull. Chem. Soc. Jpn., 43, 1883.
^[2] B. W. Erickson, et al. (1973) J. Am. Chem. Soc., 95, 3757.

関連事項

Replaces: 04-12-0068

アナリシスノート

Colour (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in DMF): -12.0 - -10.0 °
Purity (TLC(011A)): ≥ 98 %
Purity (TLC(0811)): ≥ 98 %
Assay (HPLC, area%): ≥ 99.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Solubility (1mmoll in 2ml DCM): clearly soluble
Assay (acidimetric): ≥ 95.0 %
Enantiomeric purity: ≥ 99.5 % (a/a)

To see the solvent systems used for TLC of Novabiochem^® products please click here.

法的情報

Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany

安全性情報

• 保管分類コード: 11 - Combustible Solids
• WGK: WGK 3
• 引火点(°F): Not applicable
• 引火点(℃): Not applicable