219177
4,5-Dimethylthiazole
97%
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About This Item
Prodotti consigliati
Saggio
97%
Forma fisica
powder
Indice di rifrazione
n20/D 1.521 (lit.)
P. eboll.
158 °C/742 mmHg (lit.)
Densità
1.07 g/mL at 25 °C (lit.)
Stringa SMILE
Cc1ncsc1C
InChI
1S/C5H7NS/c1-4-5(2)7-3-6-4/h3H,1-2H3
UWSONZCNXUSTKW-UHFFFAOYSA-N
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Descrizione generale
Radical bromination of 4,5-dimethylthiazole using N-bromosuccinimide in the presence of 2,2′-azobisisobutyronitrile yields mono-, tri- and tetrabromo compounds.
Applicazioni
4,5-Dimethylthiazole was used in the preparation of 4-(bromomethyl)-5-(dibromomethyl)thiazole.
Avvertenze
Danger
Indicazioni di pericolo
Consigli di prudenza
Classi di pericolo
Acute Tox. 4 Oral - Eye Dam. 1 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3
Organi bersaglio
Respiratory system
Codice della classe di stoccaggio
3 - Flammable liquids
Classe di pericolosità dell'acqua (WGK)
WGK 3
Punto d’infiammabilità (°F)
123.8 °F - closed cup
Punto d’infiammabilità (°C)
51 °C - closed cup
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The Journal of organic chemistry, 62(2), 405-410 (1997-01-24)
4-(Bromomethyl)-5-(dibromomethyl)thiazole (1) was prepared in good yields by bromination of 4,5-dimethylthiazole with 3.3 equiv of NBS in the presence of AIBN. Treatment of 1 with sodium iodide led to a thiazole o-quinodimethane 2 which was trapped in situ with dienophiles
Selective Bromination of 4, 5-Dimethylthiazole with N-Bromosuccinimide.
European Journal of Organic Chemistry, 1998(4), 593-594 (1998)
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