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Merck

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms suitable for GC

材料

分析柱

产品编号
说明
价格

SLB ®-5 ms 毛细管 GC 色谱柱

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SLB ®-5 ms 毛细管 GC 色谱柱

L × I.D. 30 m × 0.25 mm, df 0.50 μm

SLB ®-5 ms 毛细管 GC 色谱柱

L × I.D. 20 m × 0.18 mm, df 0.18 μm

標準

产品编号
说明
价格

N-亚硝基二苯胺 溶液

certified reference material, 5000 μg/mL in methanol

全氟三丁胺 (PFTBA)

analytical standard

EPA 8270 GC-MS 调谐溶液 II

certified reference material, 1000 μg/mL each component in dichloromethane

EPA CLP半挥发性校准混标 CRM

certified reference material, 1000 μg/mL each component in dichloromethane : benzene (3:1)

EPA CLP 半挥发性替代混标

certified reference material, 4000 μg/mL each component in methylene chloride

EPA 8270半挥发性内标混标

certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride, ampule of 2 × 1 mL

EPA 8270 联苯胺类混标

certified reference material, TraceCERT®, 2000 μg/mL each component in methanol, ampule of 1 mL

防護柱

产品编号
说明
价格

中等极性熔融石英管

L × I.D. 5.0 m × 0.25 mm

附屬品

产品编号
说明
价格

Wheaton wide-mouth bottle

amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 ea

Supeltex M-2B Double-Tapered Ferrule

I.D. 0.4 mm, 0.10-0.25 mm to like I.D. Column, pkg of 2 ea

毛细管柱对接连接头

body only (ferrules not included)

CONDITIONS

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

40 °C (2 min), 22 °C/min to 240 °C, 10 °C/min to 330 °C, (1 min)

inj. temp.

250 °C

MSD interface

330 °C

scan range

m/z = 40-450

carrier gas

helium, 1.0 mL/min (11 min), 10 mL/min to 1.5 mL/min (hold remainder of run)

injection

0.5 μL, splitless (0.50 min)

liner

2 mm I.D., straight

sample

50 ng on-column of a 72 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column)

说明

法律資訊

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany