G005755

GC Analysis of Basic Drugs on SLB^®-5ms (20 m x 0.18 mm I.D., 0.36 μm) after SPME using 65 μm PDMS/DVB Fiber, Fast GC Analysis

suitable for GC, application for SPME

属性

• 技術: gas chromatography (GC): suitable; solid phase microextraction (SPME): suitable
• 測試參數: sample/matrix: 500 μg/L of each compound in 2 mL 0.05M phosphate buffer, 25% sodium chloride, pH=11; SPME fiber: Polyacrylate, 85 μm (57304); PDMS/DVB Stableflex, 65 μm (57326-U); extraction: 15 min, fiber immersion in water, room temperture, stirring at 450 rpm; desorption process: 2 min, 250 °C; column: SLB-5ms, 20 m x 0.18 mm I.D., 0.36 μm (28576-U); oven: 100 °C (1 min), 20 °C/min to 325 °C (5 min); detector: MSD, m/z 40 - 450; MSD interface: 325 °C; carrier gas: helium, 1.5 mL/min, constant; liner: 0.75 mm I.D. SPME
• 適合性: application for SPME
• 應用: forensics and toxicology

说明

法律資訊

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

分析物

4-Chloro-DL-phenylalanine
Codeine
Diazepam
Heroin