技術
HPLC: suitable
測試參數
column: Ascentis Express HILlC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U)
mobile phase: [A] 5 mM ammonium formate in water, pH 6.5; [B] 5 mM ammonium formate in acetonitrile, pH 6.5; (2:98, A:B)
flow rate: 0.3 mL/min
column temp.: 35 °C
detector: ESI(+), m/z 50-400
injection: 0.1 μL
sample: 1 mg/L each in mobile phase
適合性
application for HPLC
應用
clinical
分析報告
This application demonstrates the suitability of the Ascentis Express HILIC for the analysis of omeprazole metabolites.
法律資訊
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
Omeprazole sulfone
Omeprazole
5-Hydroxyomeprazole
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