技術
gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable
測試參數
sample/matrix: amines at 5 ppm in water, 27% NaCl, pH 9.5
SPME fiber: 65 μm polydimethylsiloxane/divinylbenzene (57310)
extraction: 20 min, fiber immersed in water, rapid stirring
desorption process: 270 °C for 5 min
column: SPB®-1 SULFUR, 30 m × 0.32 mm I.D., 4.0 μm (24158)
oven: 50 °C (2 min), 10 °C/min to 150 °C
inj. temp.: 270 °C
detector: MSD, SIM at 0.6 sec/scan
carrier gas: helium, 25 cm/sec (set @ 50 °C)
liner: 0.75 mm I.D., SPME
適合性
application for SPME
應用
chemicals and industrial polymers
法律資訊
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
Triethylamine
Methylamine
Diethylamine
Dimethylamine
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