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Merck
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Key Documents

1.05635

Supelco

HPTLC plates, Silica gel 60 F₂₅₄ Multiformat pre-scored to 5 x 5 cm

glass support, plate L × W 10 cm × 10 cm

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About This Item

分類程式碼代碼:
41115711
NACRES:
NB.21

材料

glass support
silica gel 60 matrix

品質等級

特點

binder Organic Polymer
fluorescent indicator

包裝

pkg of 25 plates

技術

thin layer chromatography (TLC): suitable

層厚度

200 μm

板長度 × 寬度

10 cm × 10 cm

粒徑

5-6 μm

孔徑

60 Å medium pore diameter

儲存溫度

2-30°C

一般說明

These pre-scored glass plates fold into smaller formats with just one easy snap of the fingers.
ex Glass plates 10 x 10 cm

聯結

Replaces: 5635-5; 5635

分析報告

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m²/g
Pore volume (N₂-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 5 - 7 µm
Layer thickness: 150 - 200 µm
Deviation of layer thickness per plate: ≤ 35 µm
Chromatographic testings:
A) Colour test
hRf-values
- bleu vif organol, colour test, lipophile:
17 - 22
- Ceres Black G, colour test, lipophile: 38 - 43
- ceres Violet brn, colour test, lipophile: 58 - 64
separation number
- colourtest, lipophile:
≥ 10.0
B) Steriod test
hRf-values
- hydrocortisone, steroid test:
23 - 29
- Reichstein S, steroid test: 36 - 45
- methyltestosterone, steroid test: 43 - 52
separation number
- steroid test:
≥ 10.5
Typical value determined on a conditioned plate
Eluent A) Toluene (45% rel.humidity)
Eluent B) Ethyl acetate/Toluene (95+5 v/v; 20% rel.humidity)

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