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方案
97%
折射率
n20/D 1.451 (lit.)
沸点
175-178 °C/120 mmHg (lit.)
密度
1.021 g/mL at 25 °C (lit.)
SMILES字符串
CCOC(=O)\C(=C(/C)C)C(=O)OCC
InChI
1S/C10H16O4/c1-5-13-9(11)8(7(3)4)10(12)14-6-2/h5-6H2,1-4H3
InChI key
WEISAZNMMVPNTH-UHFFFAOYSA-N
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一般描述
Reduction of diethyl isopropylidenemalonate with sodium borohydride has been reported.
应用
Diethyl isopropylidenemalonate has been used in the synthesis of retinoids having functional groups at the side-chain terminus.
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
176.0 °F - closed cup
闪点(°C)
80 °C - closed cup
个人防护装备
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
Reduction of alkylidenecyanoacetates with sodium borohydride.
Marshall JA and Carroll RD.
The Journal of Organic Chemistry, 30(8), 2748-2754 (1965)
Y F Shealy et al.
Journal of medicinal chemistry, 31(6), 1124-1130 (1988-06-01)
Retinoids that have two functional groups at the side-chain terminus have been synthesized. The two terminal functional groups are combinations of the carboxyl, carbethoxy, and N-(ethylamino)carbonyl groups. The synthesis route is based on the sodium amide catalyzed condensation of (E,E)-beta-ionylideneacetaldehyde
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