24166
Columna para GC capilar SP®-5
L × I.D. 30 m × 0.20 mm, df 0.20 μm
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About This Item
UNSPSC Code:
41115710
eCl@ss:
32119290
Productos recomendados
material
fused silica
Quality Level
agency
meets requirements for USP G27 and G36
parameter
-60-320 °C temperature (isothermal or programmed)
Beta value
250
df
0.20 μm
technique(s)
gas chromatography (GC): suitable
L × I.D.
30 m × 0.20 mm
matrix active group
Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase
column type
capillary non-polar
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General description
Aplicación: Esta columna no polar de uso general proporciona principalmente un orden de elución por punto de ebullición con un ligero aumento en la selectividad, en especial para los compuestos aromáticos.
Código USP: Esta columna cumple los requisitos G27 y G36 de la USP .
Fase:
Código USP: Esta columna cumple los requisitos G27 y G36 de la USP .
Fase:
- Ligada
- Poli(difenil al 5 %/dimetil siloxano al 95 %)
- ≤0,32 mm D.I., <2 μm: de -60 °C a 320 °C (isotérmica o programada)
- ≤0,32 mm D.I., ≥2 μm: de -60 °C a 300 °C (isotérmica o programada)
- ≥0,53 mm D.I., <2 μm: de -60 °C a 300 °C (isotérmica ) o 320 °C (programada)
- ≥0,53 mm D.I., ≥2 μm: de -60 °C a 260 °C (isotérmica ) o 280 °C (programada)
Application
SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. It may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.
Other Notes
We offer a variety of chromatography accessories including analytical syringes
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
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P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
H J Chou
Journal of AOAC International, 81(5), 943-947 (1998-10-17)
Diethanolamine (DEA) is a precursor of N-nitrosodiethanolamine (NDELA), an animal carcinogen. A gas chromatographic (GC) method was developed for determining DEA in fatty acid diethanolamides that are commonly used in cosmetic products. Methanolic solutions of the amides were analyzed by
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave
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