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Merck
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Key Documents

34134

Supelco

B-Trichothecene mix, (DON, NIV, 3-AcDON, 15-AcDON)

~100 μg/mL in acetonitrile (each of DON, NIV, 3-AcDON and 15-AcDON), analytical standard

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About This Item

EC Number:
200-835-2
UNSPSC Code:
85151701
NACRES:
NA.24

grade

analytical standard

Quality Level

100

shelf life

limited shelf life, expiry date on the label

concentration

~100 μg/mL in acetonitrile (each of DON, NIV, 3-AcDON and 15-AcDON)

technique(s)

HPLC: suitable
gas chromatography (GC): suitable

application(s)

cleaning products
cosmetics
food and beverages
personal care

format

multi-component solution

storage temp.

−20°C

Categorías relacionadas

General description

Trichothecene mycotoxins are the largest group of toxins produced by moulds of genus Fusarium. Trichothecenes are divided into four types (A-D) according to their characteristic functional groups. The epidemiological surveys have revealed that A and B of trichothecenes are widely distributed in cereals and feed as natural pollutants. The most predominant type-B Trichothecenes are Deoxynivalenol (DON), nivalenol (NIV), 3-acetyldeoxynivalenol (3-AcDON) and 15- acetyldeoxynivalenol (15-AcDON).

Application

B-trichothecene mix may be used as reference standard in quantitative determination of type B trichothecenes using coupling liquid chromatography with tandem mass spectrometry (LC/MS/MS).
Refer to the product′s Certificate of Analysis for more information on a suitable instrument technique. Contact Technical Service for further support.

Analysis Note

purity : ≥97.0% (HPLC) for all components

pictograms

FlameExclamation mark
GHS02,GHS07

signalword

Danger

Hazard Classifications

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Eye Irrit. 2 - Flam. Liq. 2

Storage Class

3 - Flammable liquids

wgk_germany

WGK 2

flash_point_f

35.6 °F

flash_point_c

2 °C

ppe

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter

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Certificados de análisis (COA)

Lot/Batch Number
BCCL9846
BCCK9153
BCCK5089
BCCH0500
BCCG3676

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Sigma-Aldrich

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R Krska et al.
Fresenius' journal of analytical chemistry, 371(3), 285-299 (2001-11-02)
The aim of this review is to describe the state-of-the-art in the analysis of A- and B-trichothecene mycotoxins in cereals and to support knowledge and experience exchange between laboratories in the field of Fusarium mycotoxin analysis. Current screening tests and
Tomoyuki Kadota et al.
Rapid communications in mass spectrometry : RCM, 25(23), 3481-3490 (2011-11-19)
A method coupling liquid chromatography with tandem mass spectrometry (LC/MS/MS) was developed for the simultaneous quantitative determination of trichothecenes, nivalenol, deoxynivalenol, deoxynivalenol-3-glucoside, fusarenon-X, 3-acetyldeoxynivalenol, 15-acetyldeoxynivalenol, isotrichodermin, calonectrin, 3-deacetylcalonectrin, 15-deacetylcalonectrin, 3,15-diacetylnivalenol, 4,15-diacetylnivalenol, 3,15-diacetyldeoxynivalenol, and 3,4,15-triacetylnivalenol. The analytical parameters of trichothecenes and

Chromatograms

application for HPLC

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