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71478

Supelco

Nα-(2,4-Dinitro-5-fluorophenyl)-L-alaninamide

for chiral derivatization, LiChropur™, ≥99.0%

Sinonimo/i:

FDAA, Marfey’s reagent

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CHF 167.00

CHF 167.00

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CHF 167.00

About This Item

Formula empirica (notazione di Hill):
C9H9FN4O5
Numero CAS:
95713-52-3
Peso molecolare:
272.19
Beilstein:
6820069
Numero MDL:
MFCD00042049
Codice UNSPSC:
12000000
ID PubChem:
329763313
NACRES:
NA.22

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Grado

derivatization grade ((chiral))
for chiral derivatization

Livello qualitativo

100

Saggio

≥99.0% (sum of enantiomers, TLC)
≥99.0%

Stato

powder

Attività ottica

[α]20/D +56±2°, c = 1% in acetone

Purezza ottica

enantiomeric ratio: ≥99.5:0.5 (HPLC)

Qualità

LiChropur™

tecniche

HPLC: suitable

Temperatura di conservazione

2-8°C

Stringa SMILE

C[C@H](Nc1cc(F)c(cc1[N+]([O-])=O)[N+]([O-])=O)C(N)=O

InChI

1S/C9H9FN4O5/c1-4(9(11)15)12-6-2-5(10)7(13(16)17)3-8(6)14(18)19/h2-4,12H,1H3,(H2,11,15)/t4-/m0/s1
NEPLBHLFDJOJGP-BYPYZUCNSA-N

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Descrizione generale

Nα-(2,4-Dinitro-5-fluorophenyl)-L-alaninamide (FDAA) is a chiral derivatizing agent (CDA), has high enantioselectivity but low sensitivity as compared to other CDAs. It is generally used to assign the stereochemistry of amino acids in trace amounts.[1]

Applicazioni

FDAA was used as derivatizing reagent, in a study performed to understand unusual amino acids using reversed phase high performance liquid chromatography-electrospray ionization mass spectrometry (RPHPLC-ESI-MS).[1]

Altre note

Derivatization reagent for the assay of unusual chiral α-amino acid analogs[2]

Prodotti consigliati

Discover LiChropur reagents ideal for HPLC or LC-MS analysis

Note legali

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

Pittogrammi

Exclamation mark
GHS07

Avvertenze

Warning

Indicazioni di pericolo

H315,H319,H335

Classi di pericolo

Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

Organi bersaglio

Respiratory system

Codice della classe di stoccaggio

11 - Combustible Solids

Classe di pericolosità dell'acqua (WGK)

WGK 3

Punto d’infiammabilità (°F)

Not applicable

Punto d’infiammabilità (°C)

Not applicable

Dispositivi di protezione individuale

dust mask type N95 (US), Eyeshields, Gloves

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Certificati d'analisi (COA)

Lot/Batch Number
BCCN0069
BCCM9307
BCCL4997
BCCK1844
BCCH0669

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Chirality determination of unusual amino acids using precolumn derivatization and liquid chromatography-electrospray ionization mass spectrometry.
Hess S
Journal of Chromatography A, 1035(2), 211-219 (2004)
D R Goodlett et al.
Journal of chromatography. A, 707(2), 233-244 (1995-07-21)
A high-performance liquid chromatography-electrospray ionization-mass spectrometric (LC-ESI-MS) method is presented that allows rapid and accurate determination of amino acid chiral purity in a peptide. Peptides are hydrolyzed in hydrochloric acid-d1/acetic acid-d4 and then converted to diastereomers by derivatization with 1-fluoro-2,4-dinitrophenyl-5-L-alanine
Evan W Rogers et al.
Journal of natural products, 68(6), 891-896 (2005-06-25)
The absolute configurations of fistularin-3, 11-epi-fistularin-3, and a related bis-oxazolidinone were determined by microscale hydrolysis followed by derivatization with 1-fluoro-2,4-dinitrophenyl-5-l-alaninamide. Samples of fistularin-3 from Verongid marine sponges collected in the Great Barrier Reef (Australia), Baía de Todos os Santos (Brazil)
E Harth-Fritschy et al.
The journal of peptide research : official journal of the American Peptide Society, 50(6), 415-420 (1998-01-24)
Esterification of glycosylated serine and cysteine derivatives with a 4-alkoxybenzyl alcohol (Wang) resin is described. The classical methods of ester bond formation (symmetrical anhydride, 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium tetrafluoroborate [TBTU]/4-dimethylaminopyridine [DMAP] with or without 1-hydroxybenzotriazole [HOBT], pentafluorophenyl [Pfp] esters gave high percentages of
D B Goodnough et al.
Journal of chromatography. B, Biomedical applications, 672(2), 290-294 (1995-10-20)
D-Serine has recently been described to be present in the brain at high concentrations. However, while prior research has demonstrated that L-phosphoserine is the major precursor of L-serine in the brain, the possible role of D-phosphoserine as the direct precursor
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