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Documenti fondamentali

1.88051

Supelco

Water Standard

0.1%, Certified Reference Material for coulometric Karl Fischer Titration 1 g ≙ 1 mg H₂O Aquastar®

Sinonimo/i:

Acqua standard 0,1% per titolazione volumetrica Karl Fischer

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About This Item

Codice UNSPSC:
41115601
NACRES:
NA.24
Prezzi e disponibilità al momento non sono disponibili

Nome del prodotto

Acqua standard 0,1%, Certified Reference Material for coulometric Karl Fischer Titration 1 g ≙ 1 mg H₂O Aquastar®

Grado

certified reference material

Livello qualitativo

agenzia

ISO 17025, 17034

Nome Commerciale

Aquastar®

Stato

liquid

Temp. autoaccensione

287 °C (Information refers to the main component.)

Limite di esplosione

1.7-11.5 % (v/v) Information refers to the main component.)

Confezionamento

ampule of 10 × 8 mL

tecniche

Karl-Fischer titration: suitable
titration: suitable

P. ebollizione

119 °C/1013 hPa

Temp. transizione

flash point 31 °C (Information refers to the main component.)

Densità

0.92 g/cm3 at 20 °C

Formato

single component solution

Temperatura di conservazione

15-25°C

Descrizione generale

Standard del contenuto di acqua allo 0,1% preparato con approccio gravimetrico a partire da acqua e reagenti di elevata purezza. Viene caratterizzato in un laboratorio di controllo della qualità (CQ) accreditato ai sensi della norma DIN EN ISO/IEC 17025. La quantità di acqua contenuta nello standard viene determinata mediante titolazione Karl Fischer con metodo coulometrico diretto, come da ISO 760

Per avere accesso ai certificati di accreditamento attuali, siete pregati di visitare la pagina Certificazioni ISO e autovalutazioni della qualità delle sedi

Per prendere visione dei parametri certificati, compresa l′incertezza e la data di scadenza, potete scaricare il vostro certificato da http://www.sigma-aldrich.com.

Applicazioni

It is used as a certified reference material (CRM) to verify the accuracy of coulometric Karl Fischer titrators according to ISO 9001 chapter 7.1.5 “Monitoring and measuring resources”. It can also be used to check the accuracy of measured results according to European Pharmacopeia (Ph.Eur.) chapter 2.5.32 “Water Micro Determination.” Although preferable for use in coulometric method, it can be used to verify the low water content by volumetric method.

Caratteristiche e vantaggi

  • Packed in convenient 8 mL glass ampoules with 10 single-use ampoules in a box
  • Supplied with a batch-specific certificate of analysis (CoA) having data on exact measured water content of the batch, uncertainty, method of analysis, the NIST batch, and minimum shelf life
  • Misurata e convalidata in un laboratorio accreditato secondo gli standard ISO/IEC 17025 e ISO 17034
  • Directly traceable to SI unit (kg) and verified by SRM 2890 from NIST

Confezionamento

Le confezioni il cui codice SKU termina con “3”, ad es., xxxxxx1003 o xxxxxxx 4003, sono SmartChemicals e la loro etichetta è dotata di tag RFID per l′immediato trasferimento dei dati allo strumento. Ulteriori informazioni alla pagina www.sigmaaldrich.com/SmartChemicals.

Risultati analitici

Analisi (H₂O): 0,970 - 1,030 mg/g

Note legali

AQUASTAR is a registered trademark of Merck KGaA, Darmstadt, Germany

Reagente

N° Catalogo
Descrizione
Determinazione del prezzo

Pittogrammi

FlameExclamation mark

Avvertenze

Warning

Indicazioni di pericolo

Classi di pericolo

Flam. Liq. 3 - STOT SE 3

Organi bersaglio

Central nervous system

Codice della classe di stoccaggio

3 - Flammable liquids

Classe di pericolosità dell'acqua (WGK)

WGK 1

Punto d’infiammabilità (°F)

88.7 °F - closed cup - Information refers to the main ingredient.

Punto d’infiammabilità (°C)

31.5 °C - closed cup - Information refers to the main ingredient.


Certificati d'analisi (COA)

Cerca il Certificati d'analisi (COA) digitando il numero di lotto/batch corrispondente. I numeri di lotto o di batch sono stampati sull'etichetta dei prodotti dopo la parola ‘Lotto’ o ‘Batch’.

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Articoli

New Aquastar® Karl Fischer Anolyte for precise and reproducible determination of low water content in the range of 10 ppm to 10000 ppm for cells without a diaphragm.

Methods including internal extraction, external extraction, and Karl Fischer oven ensure accurate water content determination by titration.

SmartChemicals enable wireless CoA data transfer, reducing human error in titration experiments.

Protocolli

Karl Fischer titration offers accurate water content determination in hemp samples compared to the loss on drying method.

Questions

1–3 of 3 Questions  
  1. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Helpful?

  2. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

      Helpful?

  3. Can this standard be used for volumetric Karl Fischer titration?

    1 answer
    1. The water content of this standard is determined by coulometric Karl Fischer Titration according to ISO 760. Suitability for use in volumetric Karl Fischer has not been determined and analytical values reported in the Certificate of Analysis apply only to the coulometric method. The Water Standard Oven 1%, product 1.88054, is suitable for both volumetric and coulometric methods. Please see the link below to review this product option:
      https://www.sigmaaldrich.com/product/mm/188054

      Helpful?

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