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Trichloroanisole (TCA) dans le vin

Trichloroanisole (TCA) dans le vin suitable for GC, application for SPME

Matériaux

Colonne analytique

Réf. du produit
Description
Tarif

28471-U

SLB®-5ms

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Fibre SPME

Réf. du produit
Description
Tarif

57928-U

Fibres SPME Polydimethylsiloxane (PDMS)

metal alloy fiber, df 100 μm(PDMS, needle size 23 ga, for use with autosampler

Étalon

Réf. du produit
Description
Tarif

47526-U

2,4,6-Trichloroanisole solution

certified reference material, 100 μg/mL in methanol

CONDITIONS

sample/matrix

red wine spiked with 5 ppt TCA

SPME fiber

100 μm PDMS metal fiber (57928-U)

extraction

headspace, room temp (30 min)

condition

3 min. at 250 °C

desorption process

250 °C for 3 min

column

SLB®-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

60 °C (2 min), 8 °C/min to 200 °C (10 min)

MSD interface

300 °C

scan range

SIM, m/z = 195, 197, 210, 212

carrier gas

helium, 1 mL/min. constant

liner

0.75 mm I.D. SPME

Description

Informations légales

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Related Product Categories

HPLC ColumnsGC Columns & AccessoriesTLC Plates & AdsorbentsSolid Phase Microextraction (SPME)Solid Phase Extraction & QuEChERS

Related Applications

Small Molecule HPLCLarge Molecule HPLCGas Chromatography (GC)TLCSolid Phase Microextraction (SPME)Solid Phase Extraction (SPE)QuEChERS