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33065-U

Supelco

Sylon CT™

pkg of 400 mL, derivatization grade ((GC derivatization)), 5% dimethyldichlorosilane in toluene

Synonym(s):

Dichlorodimethylsilane solution, Dimethyldichlorosilane solution

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About This Item

Empirical Formula (Hill Notation):
C2H6Cl2Si
CAS Number:
75-78-5
Molecular Weight:
129.06
Beilstein/REAXYS Number:
605287
MDL number:
MFCD00000491
UNSPSC Code:
12352200
PubChem Substance ID:
329754453

grade

derivatization grade ((GC derivatization))

description

Silyl reagent

packaging

pkg of 400 mL

concentration

5% dimethyldichlorosilane in toluene

SMILES string

C[Si](C)(Cl)Cl

InChI

1S/C2H6Cl2Si/c1-5(2,3)4/h1-2H3

InChI key

LIKFHECYJZWXFJ-UHFFFAOYSA-N

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General description

For deactivating glassware.
Treat the glass tubing that you use for columns with Sylon-CT solution (5% dimethyldichlorosilane in toluene). It deactivates the tubing for use up to 350 °C to 400 °C, far exceeding the capabilities of other deactivating agents used at room temperature. Sylon CT™ also deactivates transfer lines and glass or glass-lined injection port liners. Instructions included.

Application

Sylon CT™ was used as derivatizing agent, during an experiment to develop sensitive GC method for the identification and determination of long-chain primary alkyl amines.[1] It was also used for treating Erlenmeyer flasks to prevent mycelium from sticking to the glassware during development of techniques in the identification and partial characterization the chaxamycin biosynthesis gene cluster of S. leeuwenhoekii.[2]

Legal Information

Sylon CT is a trademark of Sigma-Aldrich Co. LLC

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signalword

Danger

Hazard Classifications

Aquatic Chronic 3 - Asp. Tox. 1 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 2 - Skin Corr. 1A - STOT RE 2 - STOT SE 3

target_organs

Central nervous system

supp_hazards

EUH071

Storage Class

3 - Flammable liquids

wgk_germany

WGK 3

flash_point_f

39.2 °F - closed cup

flash_point_c

4 °C - closed cup

ppe

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

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Certificates of Analysis (COA)

Lot/Batch Number
LC23791V
LC23085V
LC21240V
LC19049V
LC17340V

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Peter Kusch et al.
Journal of chromatography. A, 1113(1-2), 198-205 (2006-02-18)
Gas chromatography with simultaneous flame-ionization detection (FID) and a nitrogen-phosphorus detection (NPD) as well as gas chromatography-mass spectrometry (GC/MS) has been used to characterize long-chain primary alkyl amines after derivatization with trifluoroacetic anhydride (TFAA). Electron impact ionization- (EI) and negative
Wonmi Ahn et al.
ACS nano, 4(7), 4181-4189 (2010-06-23)
Uniform hexagonal arrays of diverse nanotemplated metal structures were formed via selective electroless gold plating on particle-lithographed dimethyldichlorosilane layers. Surface-associated water at silica bead interstices was shown to correlate with the formation of silane rings with outer ring diameters ranging
Takehiro Fukuzaki et al.
Organic letters, 4(17), 2877-2880 (2002-08-17)
[reaction: see text] Studies on the connection between the right and left segments of azadirachtin are described. The Ireland-Claisen rearrangement of Li-enolate of the modeled ester with dichlorodimethylsilane in toluene afforded the desired limonoid framework stereoselectively in good yield.
P Mondal et al.
Talanta, 83(5), 1482-1486 (2011-01-18)
Polypyrrole nanoparticles of desired structure have been synthesized through simple micelle technique. It is then grafted with functionalized silica gel to develop a novel organic-inorganic hybrid material. The role of dimethyl dichloro silane (coupling agent) in grafting is demonstrated. The
Raimundo Ho et al.
International journal of pharmaceutics, 387(1-2), 79-86 (2009-12-17)
The sensitivity of two techniques in tracking changes in surface energetics was investigated for a crystalline excipient, D-mannitol. Macroscopic crystals of D-mannitol were grown from saturated water solution by slow cooling, and sessile drop contact angle was employed to measure
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